Ethyl-4-hydroxy-9-(4-methoxy-2,3,6-trimethylphenyl)-5,7-dimethylnona-2,7-dien-5-inoat

Base Information

Chemical Name:Ethyl-4-hydroxy-9-(4-methoxy-2,3,6-trimethylphenyl)-5,7-dimethylnona-2,7-dien-5-inoat
CAS No.:124743-95-9
Molecular Formula:C₂₃H₃₀O₄
Molecular Weight:370.489
Hs Code.:

Synonyms:Ethyl-4-hydroxy-9-(4-methoxy-2,3,6-trimethylphenyl)-5,7-dimethylnona-2,7-dien-5-inoat

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethyl-4-hydroxy-9-(4-methoxy-2,3,6-trimethylphenyl)-5,7-dimethylnona-2,7-dien-5-inoat

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Technology Process of Ethyl-4-hydroxy-9-(4-methoxy-2,3,6-trimethylphenyl)-5,7-dimethylnona-2,7-dien-5-inoat

There total 3 articles about Ethyl-4-hydroxy-9-(4-methoxy-2,3,6-trimethylphenyl)-5,7-dimethylnona-2,7-dien-5-inoat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3230-69-1
3-methyl-1-penten-4-yn-3-ol

: 124743-95-9
Ethyl-4-hydroxy-9-(4-methoxy-2,3,6-trimethylphenyl)-5,7-dimethylnona-2,7-dien-5-inoat

Guidance literature:: Multi-step reaction with 2 steps

1: MgSO₄, BF₃*Et₂O / 1 h / 5 °C

2: 1.) 1.5 M BuLi / 1.) THF/hexane, -30 deg C, 2.) THF/hexane, 2 h, room temperature

With n-butyllithium; boron trifluoride diethyl etherate; magnesium sulfate;
DOI:10.1002/hlca.19890720224

Reference yield:

: 20469-61-8
2,3,5-trimethylanisole

: 124743-95-9
Ethyl-4-hydroxy-9-(4-methoxy-2,3,6-trimethylphenyl)-5,7-dimethylnona-2,7-dien-5-inoat

Guidance literature:: Multi-step reaction with 2 steps

1: MgSO₄, BF₃*Et₂O / 1 h / 5 °C

2: 1.) 1.5 M BuLi / 1.) THF/hexane, -30 deg C, 2.) THF/hexane, 2 h, room temperature

With n-butyllithium; boron trifluoride diethyl etherate; magnesium sulfate;
DOI:10.1002/hlca.19890720224

Reference yield:

: 62054-49-3
ethyl (E)-3-formyl-2-butenoate

: 124743-94-8
2,3,5-Trimethyl-4-(3-methylpent-2-en-4-inyl)anisol

: 124743-95-9
Ethyl-4-hydroxy-9-(4-methoxy-2,3,6-trimethylphenyl)-5,7-dimethylnona-2,7-dien-5-inoat

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) THF/hexane, -30 deg C, 2.) THF/hexane, 2 h, room temperature;
DOI:10.1002/hlca.19890720224