1-O-acetyl-2-azido-2-deoxy-3,5-di-O-benzoyl-4-thio-α,β-D-arabino-pentofuranose

Base Information

Chemical Name:1-O-acetyl-2-azido-2-deoxy-3,5-di-O-benzoyl-4-thio-α,β-D-arabino-pentofuranose
CAS No.:237406-95-0
Molecular Formula:C₂₁H₁₉N₃O₆S
Molecular Weight:441.464
Hs Code.:

Synonyms:1-O-acetyl-2-azido-2-deoxy-3,5-di-O-benzoyl-4-thio-α,β-D-arabino-pentofuranose

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Chemical Property of 1-O-acetyl-2-azido-2-deoxy-3,5-di-O-benzoyl-4-thio-α,β-D-arabino-pentofuranose

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Technology Process of 1-O-acetyl-2-azido-2-deoxy-3,5-di-O-benzoyl-4-thio-α,β-D-arabino-pentofuranose

There total 4 articles about 1-O-acetyl-2-azido-2-deoxy-3,5-di-O-benzoyl-4-thio-α,β-D-arabino-pentofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 108-24-7
acetic anhydride

: 237406-94-9
methyl 2-azido-2-deoxy-3,5-di-O-benzoyl-4-thio-α,β-D-arabino-pentofuranoside

: 237406-95-0
1-O-acetyl-2-azido-2-deoxy-3,5-di-O-benzoyl-4-thio-α,β-D-arabino-pentofuranose

Guidance literature:: With sulfuric acid;
DOI:10.1080/15257779908041569

Reference yield:

: 237406-93-8
3-azido-3-deoxy-5,6-di-O,S-acetyl-1,2-O-isopropylidene-5-thio-α-D-gluco-pentofuranose

: 237406-95-0
1-O-acetyl-2-azido-2-deoxy-3,5-di-O-benzoyl-4-thio-α,β-D-arabino-pentofuranose

Guidance literature:: Multi-step reaction with 4 steps

1.1: TFA / H₂O

2.1: NaIO₄

2.2: HCl

3.1: 54 percent

4.1: 89 percent / H₂SO₄

With sodium periodate; sulfuric acid; trifluoroacetic acid; In water; 1.1: Hydrolysis / 2.1: Oxidation / 2.2: Etherification / 3.1: Esterification / 4.1: Substitution;
DOI:10.1080/15257779908041569

Reference yield:

: (2R,3S,4S)-4-Azido-2-hydroxymethyl-5-methoxy-tetrahydro-thiophen-3-ol

: 237406-95-0
1-O-acetyl-2-azido-2-deoxy-3,5-di-O-benzoyl-4-thio-α,β-D-arabino-pentofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent

2: 89 percent / H₂SO₄

With sulfuric acid; 1: Esterification / 2: Substitution;
DOI:10.1080/15257779908041569