tert-butyl cyclopent-2-ene-1-carbamate

Base Information

Chemical Name:tert-butyl cyclopent-2-ene-1-carbamate
CAS No.:144019-33-0
Molecular Formula:C₁₀H₁₇NO₂
Molecular Weight:183.25
Hs Code.:

Synonyms:tert-butyl cyclopent-2-ene-1-carbamate

Suppliers and Price of tert-butyl cyclopent-2-ene-1-carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of tert-butyl cyclopent-2-ene-1-carbamate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of tert-butyl cyclopent-2-ene-1-carbamate

There total 2 articles about tert-butyl cyclopent-2-ene-1-carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100727-30-8
2-(cyclopent-2-en-1-yl)isoindoline-1,3-dione

: 24424-99-5
di-tert-butyl dicarbonate

: 144019-33-0,153833-65-9,156731-34-9
tert-butyl cyclopent-2-ene-1-carbamate

Guidance literature:: 2-(cyclopent-2-en-1-yl)isoindoline-1,3-dione; With hydrazine hydrate; In water; at 70 ℃; for 2h;

di-tert-butyl dicarbonate; In water; at 20 ℃;

Reference yield:

: 142-29-0
cyclopentene

: 144019-33-0,153833-65-9,156731-34-9
tert-butyl cyclopent-2-ene-1-carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetra-(n-butyl)ammonium iodide; tert.-butylhydroperoxide / benzene / 12 h / 80 °C / Schlenk technique; Sealed tube

2.1: hydrazine hydrate / water / 2 h / 70 °C

2.2: 20 °C

With tert.-butylhydroperoxide; hydrazine hydrate; tetra-(n-butyl)ammonium iodide; In water; benzene;

Reference yield:

: 144019-33-0,153833-65-9,156731-34-9
tert-butyl cyclopent-2-ene-1-carbamate

: 56-86-0,21675-62-7,23009-64-5,25104-13-6,84960-48-5,25513-46-6
L-glutamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) O₃; 2.) 30percent H₂O₂ / 1.) CH₂Cl₂, -78 deg C, 7 h; 2.) CH₂Cl₂-H₂O, RT, 18 h

2: CF₃COOH / CH₂Cl₂ / 1 h / Ambient temperature

With dihydrogen peroxide; ozone; trifluoroacetic acid; In dichloromethane;
DOI:10.1002/hlca.19930760719