Ethylene Glycol Ketal of cis-3-Acetyl-6-(o-hydroxybenzoyl)-1,5,8-trihydroxytetralin 1,8-Acetonide

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Chemical Name:Ethylene Glycol Ketal of cis-3-Acetyl-6-(o-hydroxybenzoyl)-1,5,8-trihydroxytetralin 1,8-Acetonide
CAS No.:90623-87-3
Molecular Formula:C₂₄H₂₆O₇
Molecular Weight:426.466
Hs Code.:

Synonyms:Ethylene Glycol Ketal of cis-3-Acetyl-6-(o-hydroxybenzoyl)-1,5,8-trihydroxytetralin 1,8-Acetonide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethylene Glycol Ketal of cis-3-Acetyl-6-(o-hydroxybenzoyl)-1,5,8-trihydroxytetralin 1,8-Acetonide

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Technology Process of Ethylene Glycol Ketal of cis-3-Acetyl-6-(o-hydroxybenzoyl)-1,5,8-trihydroxytetralin 1,8-Acetonide

There total 6 articles about Ethylene Glycol Ketal of cis-3-Acetyl-6-(o-hydroxybenzoyl)-1,5,8-trihydroxytetralin 1,8-Acetonide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 90623-89-5
Ethylene Glycol Ketal of cis-3-Acetyl-5-methoxy-6-(o-hydroxybenzoyl)-1,8-dihydroxytetralin 1,8-Acetonide

: 90623-87-3
Ethylene Glycol Ketal of cis-3-Acetyl-6-(o-hydroxybenzoyl)-1,5,8-trihydroxytetralin 1,8-Acetonide

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium 4-mercaptobenzoate; In toluene; for 20h; Heating;
DOI:10.1021/jo00190a002

Reference yield: 27.8%

: 90641-22-8
Ethylene Glycol Ketal of cis-3-Acetyl-5-methoxy-6-(o-methoxybenzoyl)-1,8-dihydroxytetralin 1,8-Acetonide

: 90623-90-8
2-Ethyl-5,5-dimethyl-4,6,13-trioxa-benzo[de]naphthacen-8-one

: 90641-23-9
Ethylene Glycol Ketal of cis-3-Acetyl-4,5-dihydroxy-7-oxoxantho<2,3-f>tetralin 4,5-Acetonide

: 90623-87-3
Ethylene Glycol Ketal of cis-3-Acetyl-6-(o-hydroxybenzoyl)-1,5,8-trihydroxytetralin 1,8-Acetonide

: 90623-89-5
Ethylene Glycol Ketal of cis-3-Acetyl-5-methoxy-6-(o-hydroxybenzoyl)-1,8-dihydroxytetralin 1,8-Acetonide

Guidance literature:: With sodium 4-mercaptobenzoate; In N,N,N,N,N,N-hexamethylphosphoric triamide; toluene; for 18h; Further byproducts given; Heating;
DOI:10.1021/jo00190a002

Reference yield: 27.8%

: 90641-22-8
Ethylene Glycol Ketal of cis-3-Acetyl-5-methoxy-6-(o-methoxybenzoyl)-1,8-dihydroxytetralin 1,8-Acetonide

: 90641-23-9
Ethylene Glycol Ketal of cis-3-Acetyl-4,5-dihydroxy-7-oxoxantho<2,3-f>tetralin 4,5-Acetonide

: 90623-87-3
Ethylene Glycol Ketal of cis-3-Acetyl-6-(o-hydroxybenzoyl)-1,5,8-trihydroxytetralin 1,8-Acetonide

: 90641-24-0
2-[1-(2-Hydroxy-ethoxy)-ethyl]-5,5-dimethyl-4,6,13-trioxa-benzo[de]naphthacen-8-one

: 90623-89-5
Ethylene Glycol Ketal of cis-3-Acetyl-5-methoxy-6-(o-hydroxybenzoyl)-1,8-dihydroxytetralin 1,8-Acetonide

Guidance literature:: With sodium 4-mercaptobenzoate; In N,N,N,N,N,N-hexamethylphosphoric triamide; toluene; for 18h; Further byproducts given; Heating;
DOI:10.1021/jo00190a002