rac-5-(6-(1H-tetrazol-5-yl)hexyl)-2,3-di-p-tolyl-5,6,7,8-tetrahydropyrido[2,3-b]pyrazin-7-ol

Base Information

Chemical Name:rac-5-(6-(1H-tetrazol-5-yl)hexyl)-2,3-di-p-tolyl-5,6,7,8-tetrahydropyrido[2,3-b]pyrazin-7-ol
CAS No.:1447450-11-4
Molecular Formula:C₂₈H₃₃N₇O
Molecular Weight:483.616
Hs Code.:

Synonyms:rac-5-(6-(1H-tetrazol-5-yl)hexyl)-2,3-di-p-tolyl-5,6,7,8-tetrahydropyrido[2,3-b]pyrazin-7-ol

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Chemical Property of rac-5-(6-(1H-tetrazol-5-yl)hexyl)-2,3-di-p-tolyl-5,6,7,8-tetrahydropyrido[2,3-b]pyrazin-7-ol

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Technology Process of rac-5-(6-(1H-tetrazol-5-yl)hexyl)-2,3-di-p-tolyl-5,6,7,8-tetrahydropyrido[2,3-b]pyrazin-7-ol

There total 11 articles about rac-5-(6-(1H-tetrazol-5-yl)hexyl)-2,3-di-p-tolyl-5,6,7,8-tetrahydropyrido[2,3-b]pyrazin-7-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1447450-47-6
rac-(E)-5-(6-(1H-tetrazol-5-yl)hex-5-enyl)-2,3-di-p-tolyl-5,6,7,8-tetrahydropyrido[2,3-b]pyrazin-7-ol

: 1447450-11-4
rac-5-(6-(1H-tetrazol-5-yl)hexyl)-2,3-di-p-tolyl-5,6,7,8-tetrahydropyrido[2,3-b]pyrazin-7-ol

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; In ethanol; at 20 ℃; for 2h; under 262.526 Torr;

Reference yield:

: 1447450-45-4
rac-2,3-di-p-tolyl-5,6,7,8-tetrahydropyrido[2,3-b]pyrazin-7-ol

: 1447450-11-4
rac-5-(6-(1H-tetrazol-5-yl)hexyl)-2,3-di-p-tolyl-5,6,7,8-tetrahydropyrido[2,3-b]pyrazin-7-ol

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C / Inert atmosphere

2: copper(l) iodide; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / tetrahydrofuran / 20 - 40 °C

3: 5%-palladium/activated carbon; hydrogen / ethanol / 2 h / 20 °C / 262.53 Torr

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; copper(l) iodide; 5%-palladium/activated carbon; hydrogen; sodium tris(acetoxy)borohydride; In tetrahydrofuran; ethanol; 1,2-dichloro-ethane;

Reference yield:

: 764-59-0
hex-5-en-1-al

: 1447450-11-4
rac-5-(6-(1H-tetrazol-5-yl)hexyl)-2,3-di-p-tolyl-5,6,7,8-tetrahydropyrido[2,3-b]pyrazin-7-ol

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C / Inert atmosphere

2: copper(l) iodide; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / tetrahydrofuran / 20 - 40 °C

3: 5%-palladium/activated carbon; hydrogen / ethanol / 2 h / 20 °C / 262.53 Torr

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; copper(l) iodide; 5%-palladium/activated carbon; hydrogen; sodium tris(acetoxy)borohydride; In tetrahydrofuran; ethanol; 1,2-dichloro-ethane;