N-(2-hydroxy-2-(4-(5-(2-(1-phenylcyclohexyl)ethyl)-1,2,4-oxadiazol-3-yl)phenyl)ethyl)-β-alanine

Base Information

Chemical Name:N-(2-hydroxy-2-(4-(5-(2-(1-phenylcyclohexyl)ethyl)-1,2,4-oxadiazol-3-yl)phenyl)ethyl)-β-alanine
CAS No.:1356465-60-5
Molecular Formula:C₂₇H₃₃N₃O₄
Molecular Weight:463.577
Hs Code.:

Synonyms:N-(2-hydroxy-2-(4-(5-(2-(1-phenylcyclohexyl)ethyl)-1,2,4-oxadiazol-3-yl)phenyl)ethyl)-β-alanine

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Chemical Property of N-(2-hydroxy-2-(4-(5-(2-(1-phenylcyclohexyl)ethyl)-1,2,4-oxadiazol-3-yl)phenyl)ethyl)-β-alanine

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Technology Process of N-(2-hydroxy-2-(4-(5-(2-(1-phenylcyclohexyl)ethyl)-1,2,4-oxadiazol-3-yl)phenyl)ethyl)-β-alanine

There total 4 articles about N-(2-hydroxy-2-(4-(5-(2-(1-phenylcyclohexyl)ethyl)-1,2,4-oxadiazol-3-yl)phenyl)ethyl)-β-alanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: C₁₅H₁₉FO

: 1356465-64-9,1356469-64-1
(Z)-tert-butyl 3-(2-hydroxy-2-(4-(N'-hydroxycarbamimidoyl)phenyl)ethylamino)propanoate

: 1356465-60-5
N-(2-hydroxy-2-(4-(5-(2-(1-phenylcyclohexyl)ethyl)-1,2,4-oxadiazol-3-yl)phenyl)ethyl)-β-alanine

Guidance literature:: C₁₅H₁₉FO; (Z)-tert-butyl 3-(2-hydroxy-2-(4-(N'-hydroxycarbamimidoyl)phenyl)ethylamino)propanoate; With N-ethyl-N,N-diisopropylamine; at 75 ℃; for 2h;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 75 ℃;

Reference yield:

: 7598-04-1
3-(1-phenyl-cyclohexyl)-propionic acid

: 1356465-60-5
N-(2-hydroxy-2-(4-(5-(2-(1-phenylcyclohexyl)ethyl)-1,2,4-oxadiazol-3-yl)phenyl)ethyl)-β-alanine

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine; trifluoro-[1,3,5]triazine / dichloromethane / 1 h

2.1: N-ethyl-N,N-diisopropylamine / 2 h / 75 °C

2.2: 75 °C

With pyridine; trifluoro-[1,3,5]triazine; N-ethyl-N,N-diisopropylamine; In dichloromethane;

Reference yield:

: 2819-68-3
3-(2-oxo-1-phenyl-cyclohexyl)-propionic acid

: 1356465-60-5
N-(2-hydroxy-2-(4-(5-(2-(1-phenylcyclohexyl)ethyl)-1,2,4-oxadiazol-3-yl)phenyl)ethyl)-β-alanine

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide; hydrazine hydrate / ethylene glycol / 3.5 h / 130 °C / Reflux

1.2: 20 °C

2.1: pyridine; trifluoro-[1,3,5]triazine / dichloromethane / 1 h

3.1: N-ethyl-N,N-diisopropylamine / 2 h / 75 °C

3.2: 75 °C

With pyridine; trifluoro-[1,3,5]triazine; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; potassium hydroxide; In dichloromethane; ethylene glycol;