5-[p-(4-carboxylbenzylideneamino)]phenyl-10,15,20-tris(3,4,5-trimethoxyphenyl)porphyrin zinc

Base Information

Chemical Name:5-[p-(4-carboxylbenzylideneamino)]phenyl-10,15,20-tris(3,4,5-trimethoxyphenyl)porphyrin zinc
CAS No.:1424280-36-3
Molecular Formula:C₆₁H₅₁N₅O₁₁Zn
Molecular Weight:1095.49
Hs Code.:

Synonyms:5-[p-(4-carboxylbenzylideneamino)]phenyl-10,15,20-tris(3,4,5-trimethoxyphenyl)porphyrin zinc

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Chemical Property of 5-[p-(4-carboxylbenzylideneamino)]phenyl-10,15,20-tris(3,4,5-trimethoxyphenyl)porphyrin zinc

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Technology Process of 5-[p-(4-carboxylbenzylideneamino)]phenyl-10,15,20-tris(3,4,5-trimethoxyphenyl)porphyrin zinc

There total 5 articles about 5-[p-(4-carboxylbenzylideneamino)]phenyl-10,15,20-tris(3,4,5-trimethoxyphenyl)porphyrin zinc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1424280-35-2
5-(4-amidogen)phenyl-10,15,20-tris(3,4,5-trimethoxylphenyl)porphyrin zinc

: 619-66-9
4-Carboxybenzaldehyde

: 1424280-36-3
5-[p-(4-carboxylbenzylideneamino)]phenyl-10,15,20-tris(3,4,5-trimethoxyphenyl)porphyrin zinc

Guidance literature:: With acetic acid; In dichloromethane; at 38 ℃; Inert atmosphere;
DOI:10.1016/j.molstruc.2012.12.003

Reference yield:

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 1424280-36-3
5-[p-(4-carboxylbenzylideneamino)]phenyl-10,15,20-tris(3,4,5-trimethoxyphenyl)porphyrin zinc

Guidance literature:: Multi-step reaction with 4 steps

1: propionic acid / nitrobenzene / 0.75 h / 125 °C

2: tin(II) chloride dihdyrate; hydrogenchloride / water / 2.5 h / 67 °C / Inert atmosphere

3: N,N-dimethyl-formamide; chloroform / 4.5 h / Reflux

4: acetic acid / dichloromethane / 38 °C / Inert atmosphere

With hydrogenchloride; tin(II) chloride dihdyrate; acetic acid; propionic acid; In dichloromethane; chloroform; water; nitrobenzene; N,N-dimethyl-formamide;
DOI:10.1016/j.molstruc.2012.12.003

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 1424280-36-3
5-[p-(4-carboxylbenzylideneamino)]phenyl-10,15,20-tris(3,4,5-trimethoxyphenyl)porphyrin zinc

Guidance literature:: Multi-step reaction with 4 steps

1: propionic acid / nitrobenzene / 0.75 h / 125 °C

2: tin(II) chloride dihdyrate; hydrogenchloride / water / 2.5 h / 67 °C / Inert atmosphere

3: N,N-dimethyl-formamide; chloroform / 4.5 h / Reflux

4: acetic acid / dichloromethane / 38 °C / Inert atmosphere

With hydrogenchloride; tin(II) chloride dihdyrate; acetic acid; propionic acid; In dichloromethane; chloroform; water; nitrobenzene; N,N-dimethyl-formamide;
DOI:10.1016/j.molstruc.2012.12.003