3-{4-(1-imidazolylmethyl)phenyl}-2-propen-1-yl acetoacetate

Base Information

• Chemical Name: 3-{4-(1-imidazolylmethyl)phenyl}-2-propen-1-yl acetoacetate
• CAS No.: 123853-29-2
• Molecular Formula: C₁₇H₁₈N₂O₃
• Molecular Weight: 298.342
• Mol file: 123853-29-2.mol

Synonyms:3-{4-(1-imidazolylmethyl)phenyl}-2-propen-1-yl acetoacetate

Chemical Property of 3-{4-(1-imidazolylmethyl)phenyl}-2-propen-1-yl acetoacetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-{4-(1-imidazolylmethyl)phenyl}-2-propen-1-yl acetoacetate

There total 1 articles about 3-{4-(1-imidazolylmethyl)phenyl}-2-propen-1-yl acetoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-3-[4-(imidazol-1-ylmethyl)phenyl]allyl alcohol (103573-95-1) → 3-{4-(1-imidazolylmethyl)phenyl}-2-propen-1-yl acetoacetate (123853-29-2)

Guidance literature:

With triethylamine; In benzene;

Reference yield: 89.4%

3-{4-(1-imidazolylmethyl)phenyl}-2-propen-1-yl acetoacetate (123853-29-2) → (E)-3-(4-(1-imidazolylmethyl)phenyl]-2-propene-1-yl 3-aminocrotonate

Guidance literature:

With ammonium acetate; sodium hydrogencarbonate; In methanol; dichloromethane;

Reference yield:

ammonium acetate (92206-38-7) + 3-{4-(1-imidazolylmethyl)phenyl}-2-propen-1-yl acetoacetate (123853-29-2) → (E)-3-(4-(1-imidazolylmethyl)phenyl]-2-propene-1-yl 3-aminocrotonate

Guidance literature:

With sodium hydrogencarbonate; In methanol; dichloromethane;

upstream raw materials:

(E)-3-[4-(imidazol-1-ylmethyl)phenyl]allyl alcohol