Technology Process of C20H21N3O6S
There total 9 articles about C20H21N3O6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C27H37N3O6SSi;
With
lithium hydroxide; water;
In
tetrahydrofuran;
at 20 ℃;
for 3.5h;
With
hydrogenchloride; water;
In
tetrahydrofuran;
at 20 ℃;
for 3h;
With
sodium hydrogencarbonate;
In
tetrahydrofuran; water; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogenchloride / dichloromethane / 0.42 h / 0 - 20 °C
2.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / DMF (N,N-dimethyl-formamide) / 50 h / 20 °C
3.1: 2,6-dimethylpyridine / dichloromethane / 3 h / 20 °C
4.1: Burgess Reagent / 1,2-dichloro-ethane / 0.13 h / 120 °C / Microwave
5.1: lithium hydroxide; water / tetrahydrofuran / 3.5 h / 20 °C
5.2: 3 h / 20 °C
With
2,6-dimethylpyridine; hydrogenchloride; lithium hydroxide; 1-hydroxy-7-aza-benzotriazole; Burgess Reagent; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; DMF (N,N-dimethyl-formamide); dichloromethane; 1,2-dichloro-ethane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: Burgess Reagent / 1,2-dichloro-ethane / 0.13 h / 120 °C / Microwave
2.1: lithium hydroxide; water / tetrahydrofuran / 3.5 h / 20 °C
2.2: 3 h / 20 °C
With
lithium hydroxide; Burgess Reagent; water;
In
tetrahydrofuran; 1,2-dichloro-ethane;