C₇₆H₁₀₀O₁₆S

Base Information

Chemical Name:C₇₆H₁₀₀O₁₆S
CAS No.:115352-19-7
Molecular Formula:C₇₆H₁₀₀O₁₆S
Molecular Weight:1301.69
Hs Code.:

C<sub>76</sub>H<sub>100</sub>O<sub>16</sub>S

Synonyms:C₇₆H₁₀₀O₁₆S

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Chemical Property of C₇₆H₁₀₀O₁₆S

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Technology Process of C₇₆H₁₀₀O₁₆S

There total 23 articles about C₇₆H₁₀₀O₁₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104307-01-9
C₃₈H₄₈O₈Si

: 115352-19-7
C₇₆H₁₀₀O₁₆S

Guidance literature:: Multi-step reaction with 14 steps

1: 1) butyllithium / 1) ether, hexane, -42 to 0 deg C, 2) ether, hexane, -42 deg C, 10 min.

2: CrO₃*2pyridine / CH₂Cl₂ / 0.5 h / Ambient temperature

3: aluminum amalgam / tetrahydrofuran / Ambient temperature

4: sodium borohydride / ethanol / 1 h / 0 °C / further reag.: LiAlH₄, Zn(BH₄), DIBAL, B₂H₆

5: pyridinium p-toluolsulfonate / CH₂Cl₂ / Ambient temperature

6: hydrogen / palladium hydroxide on carbom / ethyl acetate / 6 h

7: 1) DMSO, oxalyl chloride, 2) triethylamine / 1) CH₂Cl₂, - 78 deg C 2) CH₂Cl₂, -78 to 0 deg C

8: 1)n-butyllithium / 1) THF, RT, 30 min, 2) THF, -78 deg C then reflux, 2 h

9: trimethylbromosilane / CH₂Cl₂ / 1) -78 deg C, 15 min, 2) -25 deg C, 30 min.

10: 60percent sodium hydride / tetrahydrofuran; dimethylformamide / 16 h / Ambient temperature

11: n-Bu₄NF / tetrahydrofuran; acetonitrile / Ambient temperature

12: 1) DMSO, oxalyl chloride, 2) triethylamine / 1) CH₂Cl₂, -78 deg C, 15 min, 2) CH₂Cl₂, -78 to 0 deg C

13: 1) sec-BuLi / 1) THF, hexane, -78 deg C, 10 min, 2) THF,hexane, -78 deg C, 20 min.

14: pyridine / 55 °C

With pyridine; sodium tetrahydroborate; n-butyllithium; oxalyl dichloride; trimethylsilyl bromide; aluminium amalgam; tetrabutyl ammonium fluoride; hydrogen; sec.-butyllithium; pyridinium p-toluenesulfonate; dipyridine chromium trioxide; sodium hydride; dimethyl sulfoxide; triethylamine; palladium hydroxide - carbon; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4020(01)86918-0

Reference yield:

: 104307-04-2
C₅₁H₇₀O₁₀Si

: 115352-19-7
C₇₆H₁₀₀O₁₆S

Guidance literature:: Multi-step reaction with 11 steps

1: sodium borohydride / ethanol / 1 h / 0 °C / further reag.: LiAlH₄, Zn(BH₄), DIBAL, B₂H₆

2: pyridinium p-toluolsulfonate / CH₂Cl₂ / Ambient temperature

3: hydrogen / palladium hydroxide on carbom / ethyl acetate / 6 h

4: 1) DMSO, oxalyl chloride, 2) triethylamine / 1) CH₂Cl₂, - 78 deg C 2) CH₂Cl₂, -78 to 0 deg C

5: 1)n-butyllithium / 1) THF, RT, 30 min, 2) THF, -78 deg C then reflux, 2 h

6: trimethylbromosilane / CH₂Cl₂ / 1) -78 deg C, 15 min, 2) -25 deg C, 30 min.

7: 60percent sodium hydride / tetrahydrofuran; dimethylformamide / 16 h / Ambient temperature

8: n-Bu₄NF / tetrahydrofuran; acetonitrile / Ambient temperature

9: 1) DMSO, oxalyl chloride, 2) triethylamine / 1) CH₂Cl₂, -78 deg C, 15 min, 2) CH₂Cl₂, -78 to 0 deg C

10: 1) sec-BuLi / 1) THF, hexane, -78 deg C, 10 min, 2) THF,hexane, -78 deg C, 20 min.

11: pyridine / 55 °C

With pyridine; sodium tetrahydroborate; n-butyllithium; oxalyl dichloride; trimethylsilyl bromide; tetrabutyl ammonium fluoride; hydrogen; sec.-butyllithium; pyridinium p-toluenesulfonate; sodium hydride; dimethyl sulfoxide; triethylamine; palladium hydroxide - carbon; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4020(01)86918-0

Reference yield:

: 104307-03-1
C₅₇H₇₆O₁₂SSi

: 115352-19-7
C₇₆H₁₀₀O₁₆S

Guidance literature:: Multi-step reaction with 13 steps

1: CrO₃*2pyridine / CH₂Cl₂ / 0.5 h / Ambient temperature

2: aluminum amalgam / tetrahydrofuran / Ambient temperature

3: sodium borohydride / ethanol / 1 h / 0 °C / further reag.: LiAlH₄, Zn(BH₄), DIBAL, B₂H₆

4: pyridinium p-toluolsulfonate / CH₂Cl₂ / Ambient temperature

5: hydrogen / palladium hydroxide on carbom / ethyl acetate / 6 h

6: 1) DMSO, oxalyl chloride, 2) triethylamine / 1) CH₂Cl₂, - 78 deg C 2) CH₂Cl₂, -78 to 0 deg C

7: 1)n-butyllithium / 1) THF, RT, 30 min, 2) THF, -78 deg C then reflux, 2 h

8: trimethylbromosilane / CH₂Cl₂ / 1) -78 deg C, 15 min, 2) -25 deg C, 30 min.

9: 60percent sodium hydride / tetrahydrofuran; dimethylformamide / 16 h / Ambient temperature

10: n-Bu₄NF / tetrahydrofuran; acetonitrile / Ambient temperature

11: 1) DMSO, oxalyl chloride, 2) triethylamine / 1) CH₂Cl₂, -78 deg C, 15 min, 2) CH₂Cl₂, -78 to 0 deg C

12: 1) sec-BuLi / 1) THF, hexane, -78 deg C, 10 min, 2) THF,hexane, -78 deg C, 20 min.

13: pyridine / 55 °C

With pyridine; sodium tetrahydroborate; n-butyllithium; oxalyl dichloride; trimethylsilyl bromide; aluminium amalgam; tetrabutyl ammonium fluoride; hydrogen; sec.-butyllithium; pyridinium p-toluenesulfonate; dipyridine chromium trioxide; sodium hydride; dimethyl sulfoxide; triethylamine; palladium hydroxide - carbon; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4020(01)86918-0