C₇₁H₉₆O₁₄

Base Information

Chemical Name:C₇₁H₉₆O₁₄
CAS No.:194039-24-2
Molecular Formula:C₇₁H₉₆O₁₄
Molecular Weight:1173.53
Hs Code.:

C<sub>71</sub>H<sub>96</sub>O<sub>14</sub>

Synonyms:C₇₁H₉₆O₁₄

Suppliers and Price of C₇₁H₉₆O₁₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₇₁H₉₆O₁₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₇₁H₉₆O₁₄

There total 35 articles about C₇₁H₉₆O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 194039-05-9
(S)-2-[(2S,6R,8S,11R)-11-Benzyloxy-8-((2S,4R)-2-tert-butyl-4-methyl-5-oxo-[1,3]dioxolan-4-ylmethyl)-4-methyl-1,7-dioxa-spiro[5.5]undec-4-en-2-yl]-propionaldehyde

: 194039-22-0
(4-{(2S,4aR,6S,8R,8aR)-8-Benzyloxy-6-[(1S,3S)-1-benzyloxy-3-((2S,3R,6S)-3-methyl-1,7-dioxa-spiro[5.5]undec-2-yl)-butyl]-2-methoxy-7-methylene-octahydro-pyrano[3,2-b]pyran-2-yl}-2-oxo-butyl)-phosphonic acid dimethyl ester

: 194039-24-2
C₇₁H₉₆O₁₄

Guidance literature:: With N-ethyl-N,N-diisopropylamine; lithium chloride; In acetonitrile;
DOI:10.1021/ja9715206

Reference yield:

: 203926-63-0
{(2S,5R,6S,8S)-5-Benzyloxy-8-[(R)-2-(4-methoxy-benzyloxy)-1-methyl-ethyl]-10-methyl-1,7-dioxa-spiro[5.5]undec-10-en-2-yl}-methanol

: 194039-24-2
C₇₁H₉₆O₁₄

Guidance literature:: Multi-step reaction with 7 steps

1: 86 percent / Dess-Martin periodinane

2: 1.) LDA / 1.) THF, hexane, -78 deg C, 20 min, 2.) THF, hexane, -78 deg C, 15 min

3: 1.) NaH

4: n-Bu₃SnH, AIBN / toluene / 2 h / 80 °C

5: 77 percent / aq. Na₂PO₄ buffer, DDQ / CH₂Cl₂; 2-methyl-propan-2-ol / 0.05 h / Irradiation

6: 90 percent / Dess-Marti periodinane, NaHCO₃ / CH₂Cl₂ / 0.5 h / Ambient temperature

7: 1.) LiCl, diisopropylethylamine / 1.) CH₃CN, RT, 10 min, 2.) CH₃CN, RT, 20 h

With 2,2'-azobis(isobutyronitrile); Na₂PO₄ buffer; tri-n-butyl-tin hydride; sodium hydride; sodium hydrogencarbonate; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium chloride; lithium diisopropyl amide; In dichloromethane; toluene; tert-butyl alcohol;
DOI:10.1021/ja973286p

Reference yield:

: 194038-95-4
{(S)-1-[(R)-2-(4-Methoxy-benzyloxy)-1-methyl-ethyl]-but-3-ynyloxy}-trimethyl-silane

: 194039-24-2
C₇₁H₉₆O₁₄

Guidance literature:: Multi-step reaction with 12 steps

1: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 20 min, 2.) THF, hexane, -78 deg C, 40 min

2: imidazole / CH₂Cl₂ / 0.75 h

3: 1.) CuI / 1.) Et₂O, from -78 to -40 deg C, 2.) Et₂O, -78 deg C, 2.5 h

4: p-TsOH*H₂O / benzene / 11 h / Ambient temperature

5: 98 percent / TBAF / tetrahydrofuran

6: 86 percent / Dess-Martin periodinane

7: 1.) LDA / 1.) THF, hexane, -78 deg C, 20 min, 2.) THF, hexane, -78 deg C, 15 min

8: 1.) NaH

9: n-Bu₃SnH, AIBN / toluene / 2 h / 80 °C

10: 77 percent / aq. Na₂PO₄ buffer, DDQ / CH₂Cl₂; 2-methyl-propan-2-ol / 0.05 h / Irradiation

11: 90 percent / Dess-Marti periodinane, NaHCO₃ / CH₂Cl₂ / 0.5 h / Ambient temperature

12: 1.) LiCl, diisopropylethylamine / 1.) CH₃CN, RT, 10 min, 2.) CH₃CN, RT, 20 h

With 1H-imidazole; copper(l) iodide; n-butyllithium; 2,2'-azobis(isobutyronitrile); Na₂PO₄ buffer; tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; sodium hydride; sodium hydrogencarbonate; Dess-Martin periodane; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium chloride; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; toluene; tert-butyl alcohol; benzene;
DOI:10.1021/ja973286p