1-benzyl-4-((1E)-3-{[(2E)-3-phenylprop-2-enyl]oxy}-prop-1-enyl)-1H-imidazole

Base Information

Chemical Name:1-benzyl-4-((1E)-3-{[(2E)-3-phenylprop-2-enyl]oxy}-prop-1-enyl)-1H-imidazole
CAS No.:1300749-17-0
Molecular Formula:C₂₂H₂₂N₂O
Molecular Weight:330.429
Hs Code.:

Synonyms:1-benzyl-4-((1E)-3-{[(2E)-3-phenylprop-2-enyl]oxy}-prop-1-enyl)-1H-imidazole

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Chemical Property of 1-benzyl-4-((1E)-3-{[(2E)-3-phenylprop-2-enyl]oxy}-prop-1-enyl)-1H-imidazole

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Technology Process of 1-benzyl-4-((1E)-3-{[(2E)-3-phenylprop-2-enyl]oxy}-prop-1-enyl)-1H-imidazole

There total 4 articles about 1-benzyl-4-((1E)-3-{[(2E)-3-phenylprop-2-enyl]oxy}-prop-1-enyl)-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: C₁₃H₁₄N₂O

: 2687-12-9
cinnamyl chloride

: 1300749-17-0
1-benzyl-4-((1E)-3-{[(2E)-3-phenylprop-2-enyl]oxy}-prop-1-enyl)-1H-imidazole

Guidance literature:: C₁₃H₁₄N₂O; With sodium hydride; In tetrahydrofuran; mineral oil; for 1h; Inert atmosphere; Cooling with ice;

cinnamyl chloride; In tetrahydrofuran; mineral oil; at 20 ℃; Inert atmosphere; Cooling with ice;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; mineral oil; at 20 ℃; Inert atmosphere;
DOI:10.1039/c0ob00657b

Reference yield:

: methyl 3-(1-benzylimidazol-4-yl)-2-propenoate

: 1300749-17-0
1-benzyl-4-((1E)-3-{[(2E)-3-phenylprop-2-enyl]oxy}-prop-1-enyl)-1H-imidazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: diisobutylaluminium hydride

2.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / Inert atmosphere; Cooling with ice

2.2: 20 °C / Inert atmosphere; Cooling with ice

2.3: 20 °C / Inert atmosphere

With sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; mineral oil;
DOI:10.1039/c0ob00657b

Reference yield:

: 104-98-3
urocanic acid

: 1300749-17-0
1-benzyl-4-((1E)-3-{[(2E)-3-phenylprop-2-enyl]oxy}-prop-1-enyl)-1H-imidazole

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid; magnesium sulfate / Reflux

2.1: sodium hydride / tetrahydrofuran

3.1: diisobutylaluminium hydride

4.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / Inert atmosphere; Cooling with ice

4.2: 20 °C / Inert atmosphere; Cooling with ice

4.3: 20 °C / Inert atmosphere

With sulfuric acid; sodium hydride; diisobutylaluminium hydride; magnesium sulfate; In tetrahydrofuran; mineral oil; 1.1: Fischer esterification;
DOI:10.1039/c0ob00657b