cis-und trans-2',6'-Dimethoxy-4'-pentyl-3-methyl-6-acetyl-1,4,5,6-tetrahydro-biphenyl

Base Information

• Chemical Name: cis-und trans-2',6'-Dimethoxy-4'-pentyl-3-methyl-6-acetyl-1,4,5,6-tetrahydro-biphenyl
• CAS No.: 14132-53-7
• Molecular Formula: C₂₂H₃₂O₃
• Molecular Weight: 344.494

Synonyms:cis-und trans-2',6'-Dimethoxy-4'-pentyl-3-methyl-6-acetyl-1,4,5,6-tetrahydro-biphenyl

Chemical Property of cis-und trans-2',6'-Dimethoxy-4'-pentyl-3-methyl-6-acetyl-1,4,5,6-tetrahydro-biphenyl

Chemical Property:

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Technology Process of cis-und trans-2',6'-Dimethoxy-4'-pentyl-3-methyl-6-acetyl-1,4,5,6-tetrahydro-biphenyl

There total 3 articles about cis-und trans-2',6'-Dimethoxy-4'-pentyl-3-methyl-6-acetyl-1,4,5,6-tetrahydro-biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

2-[(E)-2-(2,6-Dimethoxy-4-pentyl-phenyl)-vinyl]-2,6-dimethyl-3,4-dihydro-2H-pyran (93503-47-0,93503-48-1) → cis-und trans-2',6'-Dimethoxy-4'-pentyl-3-methyl-6-acetyl-1,4,5,6-tetrahydro-biphenyl (14132-53-7)

Guidance literature:

In dichloromethane; for 48h; Ambient temperature;

DOI:10.1021/jo00200a061

Reference yield:

(2,6-Dimethoxy-4-pentyl-benzylidene)-triphenyl-λ5-phosphane (93503-49-2) → cis-und trans-2',6'-Dimethoxy-4'-pentyl-3-methyl-6-acetyl-1,4,5,6-tetrahydro-biphenyl (14132-53-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 1. Diisobutylaluminium hydride

2: 94 percent / CH₂Cl₂ / 48 h / Ambient temperature

With diisobutylaluminium hydride; In dichloromethane;

DOI:10.1021/jo00200a061

Reference yield:

→ cis-und trans-2',6'-Dimethoxy-4'-pentyl-3-methyl-6-acetyl-1,4,5,6-tetrahydro-biphenyl (14132-53-7)

Guidance literature:

1-(2',6'-Dimethoxy-4'-n-pentylphenyl)-3-methyl-butadien in Bzl., Methylvinylketon (Hydrochinon, 100grad, Druck);

upstream raw materials:

2-[(E)-2-(2,6-Dimethoxy-4-pentyl-phenyl)-vinyl]-2,6-dimethyl-3,4-dihydro-2H-pyran

(2,6-Dimethoxy-4-pentyl-benzylidene)-triphenyl-λ⁵-phosphane

Downstream raw materials:

cis-DL-Cannabidiol-dimethylether

(6aR,10aR)-1-Methoxy-6,6,9-trimethyl-3-pentyl-6a,7,8,10a-tetrahydro-6H-benzo[c]chromene

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