N-{2-[cyano-(triphenyl-λ⁵-phosphanylidene)-methyl]-4-phenyl-thiazol-5-yl}-4-methyl-benzamide

Base Information

• Chemical Name: N-{2-[cyano-(triphenyl-λ⁵-phosphanylidene)-methyl]-4-phenyl-thiazol-5-yl}-4-methyl-benzamide
• CAS No.: 442513-27-1
• Molecular Formula: C₃₇H₂₈N₃OPS
• Molecular Weight: 593.689

Synonyms:N-{2-[cyano-(triphenyl-λ⁵-phosphanylidene)-methyl]-4-phenyl-thiazol-5-yl}-4-methyl-benzamide

Chemical Property of N-{2-[cyano-(triphenyl-λ⁵-phosphanylidene)-methyl]-4-phenyl-thiazol-5-yl}-4-methyl-benzamide

Chemical Property:

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Technology Process of N-{2-[cyano-(triphenyl-λ⁵-phosphanylidene)-methyl]-4-phenyl-thiazol-5-yl}-4-methyl-benzamide

There total 1 articles about N-{2-[cyano-(triphenyl-λ⁵-phosphanylidene)-methyl]-4-phenyl-thiazol-5-yl}-4-methyl-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

(cyano)thiocarbamoylmethylenotriphenylphosphorane (171360-65-9) + N-(1-chloro-2-oxo-2-phenyl-ethyl)-4-methyl-benzamide → N-{2-[cyano-(triphenyl-λ5-phosphanylidene)-methyl]-4-phenyl-thiazol-5-yl}-4-methyl-benzamide (442513-27-1)

Guidance literature:

With triethylamine; In acetonitrile; at 20 ℃; for 24h;

DOI:10.1023/A:1013986223340

Reference yield: 86.0%

N-{2-[cyano-(triphenyl-λ5-phosphanylidene)-methyl]-4-phenyl-thiazol-5-yl}-4-methyl-benzamide (442513-27-1) → N-(2-cyanomethyl-4-phenyl-thiazol-5-yl)-4-methyl-benzamide

Guidance literature:

With acetyl chloride; In acetic acid; at 20 - 25 ℃; for 0.333333h;

DOI:10.1023/A:1013986223340

Reference yield: 72.0%

N-{2-[cyano-(triphenyl-λ5-phosphanylidene)-methyl]-4-phenyl-thiazol-5-yl}-4-methyl-benzamide (442513-27-1) → 2-methoxycarbonylmethyl-5-p-toluoylamino-4-phenylthiazole

Guidance literature:

N-{2-[cyano-(triphenyl-λ⁵-phosphanylidene)-methyl]-4-phenyl-thiazol-5-yl}-4-methyl-benzamide; With hydrogenchloride; In methanol; for 0.333333h;

In methanol; water; at 20 ℃; for 1h;

DOI:10.1023/A:1013986223340

upstream raw materials:

(cyano)thiocarbamoylmethylenotriphenylphosphorane

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