4-methyl-4'-iodostilbene

Base Information

Chemical Name:4-methyl-4'-iodostilbene
CAS No.:57083-01-9
Molecular Formula:C₁₅H₁₃I
Molecular Weight:320.173
Hs Code.:

Synonyms:4-methyl-4'-iodostilbene

Suppliers and Price of 4-methyl-4'-iodostilbene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methyl-4'-iodostilbene

Chemical Property:

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Technology Process of 4-methyl-4'-iodostilbene

There total 8 articles about 4-methyl-4'-iodostilbene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 16004-15-2
1-bromomethyl-4-iodobenzene

: 104-87-0
4-methyl-benzaldehyde

: 57083-01-9
4-methyl-4'-iodostilbene

Guidance literature:: 1-bromomethyl-4-iodobenzene; With phosphorous acid trimethyl ester; for 4h; Heating;

With sodium methylate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; at 20 ℃; for 1.5h;

4-methyl-benzaldehyde; With sodium methylate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; at 20 ℃; for 21h;
DOI:10.1002/chem.200401313

Reference yield:

: phosphorous acid 4-iodo-benzyl ester dimethyl ester

: 104-87-0
4-methyl-benzaldehyde

: 57083-01-9
4-methyl-4'-iodostilbene

Guidance literature:: phosphorous acid 4-iodo-benzyl ester dimethyl ester; With sodium methylate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; at 20 ℃; for 1.5h;

4-methyl-benzaldehyde; With sodium methylate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; for 18h;
DOI:10.1002/chem.200500415

Reference yield:

: 16004-15-2
1-bromomethyl-4-iodobenzene

: 57083-01-9
4-methyl-4'-iodostilbene

Guidance literature:: Multi-step reaction with 2 steps

1.1: 4 h / Heating

2.1: NaOMe / dimethylformamide; tetrahydrofuran; methanol / 1.5 h / 20 °C

2.2: 18.1 g / NaOMe / dimethylformamide; tetrahydrofuran; methanol / 18 h

With sodium methylate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1002/chem.200500415