6-{[5'-({6-[(5'-azidomethyl-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]e-5-carbonyl)-amino]-hexanoylamino}-methyl)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]e-5-carbonyl]-amino}-hexanoic acid pentafluorophenyl ester

Base Information

Chemical Name:6-{[5'-({6-[(5'-azidomethyl-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]e-5-carbonyl)-amino]-hexanoylamino}-methyl)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]e-5-carbonyl]-amino}-hexanoic acid pentafluorophenyl ester
CAS No.:669693-45-2
Molecular Formula:C₄₂H₅₉F₅N₆O₁₃
Molecular Weight:950.955
Hs Code.:

6-{[5'-({6-[(5'-azidomethyl-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]e-5-carbonyl)-amino]-hexanoylamino}-methyl)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]e-5-carbonyl]-amino}-hexanoic acid pentafluorophenyl ester

Synonyms:6-{[5'-({6-[(5'-azidomethyl-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]e-5-carbonyl)-amino]-hexanoylamino}-methyl)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]e-5-carbonyl]-amino}-hexanoic acid pentafluorophenyl ester

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Chemical Property of 6-{[5'-({6-[(5'-azidomethyl-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]e-5-carbonyl)-amino]-hexanoylamino}-methyl)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]e-5-carbonyl]-amino}-hexanoic acid pentafluorophenyl ester

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Technology Process of 6-{[5'-({6-[(5'-azidomethyl-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]e-5-carbonyl)-amino]-hexanoylamino}-methyl)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]e-5-carbonyl]-amino}-hexanoic acid pentafluorophenyl ester

There total 7 articles about 6-{[5'-({6-[(5'-azidomethyl-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]e-5-carbonyl)-amino]-hexanoylamino}-methyl)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]e-5-carbonyl]-amino}-hexanoic acid pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 6-{[(4S,5S,4'R,5'R)-5'-({6-[((4S,5S,4'R,5'R)-5'-Azidomethyl-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]e-5-carbonyl)-amino]-hexanoylamino}-methyl)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]e-5-carbonyl]-amino}-hexanoic acid

: 669693-45-2
6-{[5'-({6-[(5'-azidomethyl-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]e-5-carbonyl)-amino]-hexanoylamino}-methyl)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]e-5-carbonyl]-amino}-hexanoic acid pentafluorophenyl ester

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane;
DOI:10.1016/j.tetlet.2003.10.105

Reference yield:

: 201340-96-7
6-azido-6-deoxy-2,3-O-isopropylidene-D-mannono-1,4-lactone

: 669693-45-2
6-{[5'-({6-[(5'-azidomethyl-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]e-5-carbonyl)-amino]-hexanoylamino}-methyl)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]e-5-carbonyl]-amino}-hexanoic acid pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 6 steps

1.1: 96 percent / diisopropylethylamine

2.1: 90 percent / p-toluenesulfonic acid

3.1: hydrogen / palladium black / dioxane

4.1: 90 percent / diisopropylethylamine; O-(1H-benzotriazol-yl)-N,N,N",N"-tetramethyluronium BF₄^(1-)

5.1: aq. sodium hydroxide / dioxane

5.2: Amberlite IR-120 H+

6.1: 90 percent / EDCI / dioxane

With sodium hydroxide; hydrogen; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; palladium; In 1,4-dioxane;
DOI:10.1016/j.tetlet.2003.10.105

Reference yield:

: 669693-35-0
6-{[(4S,5S)-5-((1R,2R)-3-Azido-1,2-dihydroxy-propyl)-2,2-dimethyl-[1,3]dioxolane-4-carbonyl]-amino}-hexanoic acid methyl ester

: 669693-45-2
6-{[5'-({6-[(5'-azidomethyl-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]e-5-carbonyl)-amino]-hexanoylamino}-methyl)-2,2,2',2'-tetramethyl-[4,4']bi[[1,3]dioxolanyl]e-5-carbonyl]-amino}-hexanoic acid pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: 90 percent / p-toluenesulfonic acid

2.1: hydrogen / palladium black / dioxane

3.1: 90 percent / diisopropylethylamine; O-(1H-benzotriazol-yl)-N,N,N",N"-tetramethyluronium BF₄^(1-)

4.1: aq. sodium hydroxide / dioxane

4.2: Amberlite IR-120 H+

5.1: 90 percent / EDCI / dioxane

With sodium hydroxide; hydrogen; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; palladium; In 1,4-dioxane;
DOI:10.1016/j.tetlet.2003.10.105