12-(tert-butoxycarbonyl)-6,12-bis(-benzyloxy)-7-oxo-6,12-diazadodecanenitrile

Base Information

Chemical Name:12-(tert-butoxycarbonyl)-6,12-bis(-benzyloxy)-7-oxo-6,12-diazadodecanenitrile
CAS No.:144108-55-4
Molecular Formula:C₂₉H₃₉N₃O₅
Molecular Weight:509.646
Hs Code.:

Synonyms:12-(tert-butoxycarbonyl)-6,12-bis(-benzyloxy)-7-oxo-6,12-diazadodecanenitrile

Suppliers and Price of 12-(tert-butoxycarbonyl)-6,12-bis(-benzyloxy)-7-oxo-6,12-diazadodecanenitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 12-(tert-butoxycarbonyl)-6,12-bis(-benzyloxy)-7-oxo-6,12-diazadodecanenitrile

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 12-(tert-butoxycarbonyl)-6,12-bis(-benzyloxy)-7-oxo-6,12-diazadodecanenitrile

There total 3 articles about 12-(tert-butoxycarbonyl)-6,12-bis(-benzyloxy)-7-oxo-6,12-diazadodecanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1575-61-7
5-Chlorovaleroyl chloride

: 144108-55-4
12-(tert-butoxycarbonyl)-6,12-bis(-benzyloxy)-7-oxo-6,12-diazadodecanenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / 1 N NaOH / CH₂Cl₂ / Ambient temperature

2: 1.) NaH / 1.) DMF, 0 deg C, 30 min, 2.) 80 deg C, overnight

With sodium hydroxide; sodium hydride; In dichloromethane;
DOI:10.1021/jm00103a012

Reference yield:

: 112139-59-0
O-benzyl-N-(4-cyanobutyl)-hydroxylamine

: 144108-55-4
12-(tert-butoxycarbonyl)-6,12-bis(-benzyloxy)-7-oxo-6,12-diazadodecanenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / 1 N NaOH / CH₂Cl₂ / Ambient temperature

2: 1.) NaH / 1.) DMF, 0 deg C, 30 min, 2.) 80 deg C, overnight

With sodium hydroxide; sodium hydride; In dichloromethane;
DOI:10.1021/jm00103a012

Reference yield:

: 79722-21-7
tert-butyl N-(benzyloxy)carbamate

: 144108-54-3
N-(benzyloxy)-N-(4-cyanobutyl)-5-chloropentanamide

: 144108-55-4
12-(tert-butoxycarbonyl)-6,12-bis(-benzyloxy)-7-oxo-6,12-diazadodecanenitrile

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMF, 0 deg C, 30 min, 2.) 80 deg C, overnight;
DOI:10.1021/jm00103a012