4-(3-(2,3,5-trimethylcyclopenta-1,4-diene)-4-(cyclohexylamino)benzyl)-2-(2,3,5-trimethylcyclopenta-1,4-diene)-N-cyclohexylbenzeneamine

Base Information

Chemical Name:4-(3-(2,3,5-trimethylcyclopenta-1,4-diene)-4-(cyclohexylamino)benzyl)-2-(2,3,5-trimethylcyclopenta-1,4-diene)-N-cyclohexylbenzeneamine
CAS No.:959641-02-2
Molecular Formula:C₄₁H₅₄N₂
Molecular Weight:574.893
Hs Code.:

Synonyms:4-(3-(2,3,5-trimethylcyclopenta-1,4-diene)-4-(cyclohexylamino)benzyl)-2-(2,3,5-trimethylcyclopenta-1,4-diene)-N-cyclohexylbenzeneamine

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Chemical Property of 4-(3-(2,3,5-trimethylcyclopenta-1,4-diene)-4-(cyclohexylamino)benzyl)-2-(2,3,5-trimethylcyclopenta-1,4-diene)-N-cyclohexylbenzeneamine

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Technology Process of 4-(3-(2,3,5-trimethylcyclopenta-1,4-diene)-4-(cyclohexylamino)benzyl)-2-(2,3,5-trimethylcyclopenta-1,4-diene)-N-cyclohexylbenzeneamine

There total 1 articles about 4-(3-(2,3,5-trimethylcyclopenta-1,4-diene)-4-(cyclohexylamino)benzyl)-2-(2,3,5-trimethylcyclopenta-1,4-diene)-N-cyclohexylbenzeneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 943406-22-2
4-(3-(3,4-dimethylcyclopenta-1,3-dienone)-4-(cyclohexylamino)benzyl)-2-(3,4-dimethylcyclopenta-1,3-dienone)-N-cyclohexylbenzeneamine

: 917-54-4
methyllithium

: 959641-02-2
4-(3-(2,3,5-trimethylcyclopenta-1,4-diene)-4-(cyclohexylamino)benzyl)-2-(2,3,5-trimethylcyclopenta-1,4-diene)-N-cyclohexylbenzeneamine

Guidance literature:: methyllithium; With cerium(III) chloride; In tetrahydrofuran; at -78 ℃; for 1h;

4-(3-(3,4-dimethylcyclopenta-1,3-dienone)-4-(cyclohexylamino)benzyl)-2-(3,4-dimethylcyclopenta-1,3-dienone)-N-cyclohexylbenzeneamine; In tetrahydrofuran; at -78 ℃; for 2h;

Reference yield: 100.0%

: 959641-02-2
4-(3-(2,3,5-trimethylcyclopenta-1,4-diene)-4-(cyclohexylamino)benzyl)-2-(2,3,5-trimethylcyclopenta-1,4-diene)-N-cyclohexylbenzeneamine

: 4-(3-(2,3,5-trimethylcyclopentadienyl)-4-(cyclohexylamido)benzyl)-2-(2,3,5-tri-methylcyclopentadienyl)-N-cyclohexylbenzeneamido tetralithium salt

Guidance literature:: With n-butyllithium; In diethyl ether; hexane; at -30 ℃; for 12h;

Reference yield: 87.0%

: tetrakis(dimethylamido)titanium(IV)

: 959641-02-2
4-(3-(2,3,5-trimethylcyclopenta-1,4-diene)-4-(cyclohexylamino)benzyl)-2-(2,3,5-trimethylcyclopenta-1,4-diene)-N-cyclohexylbenzeneamine

: 75-78-5,30107-43-8
dimethylsilicon dichloride

: 4,4'-CH2[[2-η5-2,3,5-Me3C5H)C6H3NC6H11-κN]Ti(IV)Cl2]2

Guidance literature:: tetrakis(dimethylamido)titanium(IV); 4-(3-(2,3,5-trimethylcyclopenta-1,4-diene)-4-(cyclohexylamino)benzyl)-2-(2,3,5-trimethylcyclopenta-1,4-diene)-N-cyclohexylbenzeneamine; In toluene; at 80 ℃; for 48h;

dimethylsilicon dichloride; In toluene; at 20 ℃; for 4h;