N'-(9-anthracenylidene)benzothiohydrazide

Base Information

• Chemical Name: N'-(9-anthracenylidene)benzothiohydrazide
• CAS No.: 339117-45-2
• Molecular Formula: C₂₂H₁₆N₂S
• Molecular Weight: 340.448
• Mol file: 339117-45-2.mol

Synonyms:N'-(9-anthracenylidene)benzothiohydrazide

Chemical Property of N'-(9-anthracenylidene)benzothiohydrazide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of N'-(9-anthracenylidene)benzothiohydrazide

There total 1 articles about N'-(9-anthracenylidene)benzothiohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

thiobenzoylhydrazine (20605-40-7) + 9-anthracene aldehyde (642-31-9) → N'-(9-anthracenylidene)benzothiohydrazide (339117-45-2)

Guidance literature:

With acetic acid; In methanol;

DOI:10.1016/j.jorganchem.2016.09.032

Reference yield: 85.6%

N'-(9-anthracenylidene)benzothiohydrazide (339117-45-2) + triethyl gallium (1115-99-7) → diethyl[N-(9-anthryl)methylenethiobenzahydrazonato]gallium

Guidance literature:

In cyclohexane; benzene; under N2, soln. of GaCl3 (2 mmol) in cyclohexane added with stirring to soln. of ligand (2 mmol) in cyclohexane/benzene (5/1), stirred for 30 min at room temp.; evapd. (vac.), recrystd. (benzene), elem. anal.;

DOI:10.1016/j.ica.2006.08.041

Reference yield: 75.0%

N'-(9-anthracenylidene)benzothiohydrazide (339117-45-2) + palladium dichloride → C88H56N8Pd4S4

Guidance literature:

With sodium acetate; lithium chloride; In methanol; at 24.84 ℃; for 48h;

DOI:10.1016/j.jorganchem.2016.09.032

upstream raw materials:

thiobenzoylhydrazine

9-anthracene aldehyde

Downstream raw materials:

cis-[Ru(PPh₃)₂(HL²)_2]