(2S,3S)-2,3-Bis-benzoyloxy-3-carboxy-propionatebenzyl-isopropyl-methyl-phenyl-phosphonium;

Base Information

Chemical Name:(2S,3S)-2,3-Bis-benzoyloxy-3-carboxy-propionatebenzyl-isopropyl-methyl-phenyl-phosphonium;
CAS No.:84673-91-6
Molecular Formula:C₁₇H₂₂P*C₁₈H₁₃O₈
Molecular Weight:614.632
Hs Code.:

Synonyms:(2S,3S)-2,3-Bis-benzoyloxy-3-carboxy-propionatebenzyl-isopropyl-methyl-phenyl-phosphonium;

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Chemical Property of (2S,3S)-2,3-Bis-benzoyloxy-3-carboxy-propionatebenzyl-isopropyl-methyl-phenyl-phosphonium;

Chemical Property:

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Technology Process of (2S,3S)-2,3-Bis-benzoyloxy-3-carboxy-propionatebenzyl-isopropyl-methyl-phenyl-phosphonium;

There total 3 articles about (2S,3S)-2,3-Bis-benzoyloxy-3-carboxy-propionatebenzyl-isopropyl-methyl-phenyl-phosphonium; which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 17026-42-5
O,O'-dibenzoyl-D-tartaric acid

: Benzylidene-isopropyl-methyl-phenyl-λ⁵-phosphane

: 84673-91-6
(2S,3S)-2,3-Bis-benzoyloxy-3-carboxy-propionatebenzyl-isopropyl-methyl-phenyl-phosphonium;

Guidance literature:: In tetrahydrofuran; for 12h;

Reference yield:

: 51290-74-5
Dibenzylmethylphenylphosphonium-iodid

: 84673-91-6
(2S,3S)-2,3-Bis-benzoyloxy-3-carboxy-propionatebenzyl-isopropyl-methyl-phenyl-phosphonium;

Guidance literature:: Multi-step reaction with 3 steps

1: 1) LiAlH₄, 20percent Na-K-tartrate / 1) THF, 2) MeCN, reflux

2: NaNH₂ / tetrahydrofuran / 1 h / Heating

3: 41 percent / tetrahydrofuran / 12 h

With lithium aluminium tetrahydride; Rochelle's salt; sodium amide; In tetrahydrofuran;

Reference yield:

: 24153-77-3
(R,S)-Benzylisopropylmethylphenylphosphonium-bromid

: 84673-91-6
(2S,3S)-2,3-Bis-benzoyloxy-3-carboxy-propionatebenzyl-isopropyl-methyl-phenyl-phosphonium;

Guidance literature:: Multi-step reaction with 2 steps

1: NaNH₂ / tetrahydrofuran / 1 h / Heating

2: 41 percent / tetrahydrofuran / 12 h

With sodium amide; In tetrahydrofuran;