(5S)-5-{4-[2-(5-ethylpyridin-2-yl)ethoxy]benzyl}-(5-⁽²⁾H)-1,3-thiazolidine-2,4-dione trifluoroacetate

Base Information

• Chemical Name: (5S)-5-{4-[2-(5-ethylpyridin-2-yl)ethoxy]benzyl}-(5-⁽²⁾H)-1,3-thiazolidine-2,4-dione trifluoroacetate
• CAS No.: 1259829-16-7
• Molecular Formula: C₂HF₃O₂*C₁₉H₂₀N₂O₃S
• Molecular Weight: 471.461

Synonyms:(5S)-5-{4-[2-(5-ethylpyridin-2-yl)ethoxy]benzyl}-(5-⁽²⁾H)-1,3-thiazolidine-2,4-dione trifluoroacetate

Chemical Property of (5S)-5-{4-[2-(5-ethylpyridin-2-yl)ethoxy]benzyl}-(5-⁽²⁾H)-1,3-thiazolidine-2,4-dione trifluoroacetate

Chemical Property:

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Technology Process of (5S)-5-{4-[2-(5-ethylpyridin-2-yl)ethoxy]benzyl}-(5-⁽²⁾H)-1,3-thiazolidine-2,4-dione trifluoroacetate

There total 1 articles about (5S)-5-{4-[2-(5-ethylpyridin-2-yl)ethoxy]benzyl}-(5-⁽²⁾H)-1,3-thiazolidine-2,4-dione trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+/-)-5-{4-[2-(5-ethylpyridin-2-yl)ethoxy]benzyl}-(5-(2)H)-1,3-thiazolidine-2,4-dione hydrochloride (1259829-13-4) + trifluoroacetic acid (76-05-1) → (5R)-5-{4-[2-(5-ethylpyridin-2-yl)ethoxy]benzyl}-(5-(2)H)-1,3-thiazolidine-2,4-dione trifluoroacetate (1259829-20-3) + (5S)-5-{4-[2-(5-ethylpyridin-2-yl)ethoxy]benzyl}-(5-(2)H)-1,3-thiazolidine-2,4-dione trifluoroacetate (1259829-16-7)

Guidance literature:

With CHIRALPAK IA; In ethanol; Resolution of racemate;

Reference yield: 80.0%

(5S)-5-{4-[2-(5-ethylpyridin-2-yl)ethoxy]benzyl}-(5-(2)H)-1,3-thiazolidine-2,4-dione trifluoroacetate (1259829-16-7) → (5S)-5-{4-[2-(5-ethylpyridin-2-yl)ethoxy]benzyl}-(5-(2)H)-1,3-thiazolidine-2,4-dione hydrochloride (1259828-69-7)

Guidance literature:

(5S)-5-{4-[2-(5-ethylpyridin-2-yl)ethoxy]benzyl}-(5-⁽²⁾H)-1,3-thiazolidine-2,4-dione trifluoroacetate; In deuteromethanol; at 20 ℃; for 2h;

With hydrogenchloride; In methanol; deuteromethanol; at 20 ℃; for 0.5h;

upstream raw materials:

(+/-)-5-{4-[2-(5-ethylpyridin-2-yl)ethoxy]benzyl}-(5-⁽²⁾H)-1,3-thiazolidine-2,4-dione hydrochloride

trifluoroacetic acid

Downstream raw materials:

(5S)-5-{4-[2-(5-ethylpyridin-2-yl)ethoxy]benzyl}-(5-⁽²⁾H)-1,3-thiazolidine-2,4-dione hydrochloride

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