(3aR-(3aα,4α,6aα))-tetrahydro-2,2-dimethyl-4-[2-(2-phenyl-1,3-dioxolan-2-yl)phenyl]furo[3,4-d]-1,3-dioxole

Base Information

Chemical Name:(3aR-(3aα,4α,6aα))-tetrahydro-2,2-dimethyl-4-[2-(2-phenyl-1,3-dioxolan-2-yl)phenyl]furo[3,4-d]-1,3-dioxole
CAS No.:185699-83-6
Molecular Formula:C₂₂H₂₄O₅
Molecular Weight:368.43
Hs Code.:

Synonyms:(3aR-(3aα,4α,6aα))-tetrahydro-2,2-dimethyl-4-[2-(2-phenyl-1,3-dioxolan-2-yl)phenyl]furo[3,4-d]-1,3-dioxole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3aR-(3aα,4α,6aα))-tetrahydro-2,2-dimethyl-4-[2-(2-phenyl-1,3-dioxolan-2-yl)phenyl]furo[3,4-d]-1,3-dioxole

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Technology Process of (3aR-(3aα,4α,6aα))-tetrahydro-2,2-dimethyl-4-[2-(2-phenyl-1,3-dioxolan-2-yl)phenyl]furo[3,4-d]-1,3-dioxole

There total 3 articles about (3aR-(3aα,4α,6aα))-tetrahydro-2,2-dimethyl-4-[2-(2-phenyl-1,3-dioxolan-2-yl)phenyl]furo[3,4-d]-1,3-dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 185699-82-5
[4R-(4α[R^*],5α)]-2,2-dimethyl-α⁴-[2-(2-phenyl-1,3-dioxolan-2-yl)phenyl]-1,3-dioxolane-4,5-dimethanol

: 185699-83-6
(3aR-(3aα,4α,6aα))-tetrahydro-2,2-dimethyl-4-[2-(2-phenyl-1,3-dioxolan-2-yl)phenyl]furo[3,4-d]-1,3-dioxole

Guidance literature:: With pyridine; p-toluenesulfonyl chloride; for 144h; Ambient temperature;
DOI:10.1021/jo961372m

Reference yield:

: 23262-84-2
2,3-O-isopropylidene-β-L-erythrofuranose

: 185699-83-6
(3aR-(3aα,4α,6aα))-tetrahydro-2,2-dimethyl-4-[2-(2-phenyl-1,3-dioxolan-2-yl)phenyl]furo[3,4-d]-1,3-dioxole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) MgCl₂, KI, K / 1.) THF, room temperature, 3 h, 2.) THF, room temperature, 18 h

2: 100 percent / tosyl chloride, pyridine / 144 h / Ambient temperature

With pyridine; p-toluenesulfonyl chloride; potassium iodide; magnesium chloride;
DOI:10.1021/jo961372m

Reference yield:

: 78105-68-7
2-(2-bromophenyl)-2-phenyl-1,3-dioxolane

: 185699-83-6
(3aR-(3aα,4α,6aα))-tetrahydro-2,2-dimethyl-4-[2-(2-phenyl-1,3-dioxolan-2-yl)phenyl]furo[3,4-d]-1,3-dioxole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) MgCl₂, KI, K / 1.) THF, room temperature, 3 h, 2.) THF, room temperature, 18 h

2: 100 percent / tosyl chloride, pyridine / 144 h / Ambient temperature

With pyridine; p-toluenesulfonyl chloride; potassium iodide; magnesium chloride;
DOI:10.1021/jo961372m