4-chloro-N-(pyridin-2-ylmethyl)-N-[4-(1H-tetrazol-5-yl)benzyl]benzenesulfonamide

Base Information

Chemical Name:4-chloro-N-(pyridin-2-ylmethyl)-N-[4-(1H-tetrazol-5-yl)benzyl]benzenesulfonamide
CAS No.:1191066-20-2
Molecular Formula:C₂₀H₁₇ClN₆O₂S
Molecular Weight:440.913
Hs Code.:

Synonyms:4-chloro-N-(pyridin-2-ylmethyl)-N-[4-(1H-tetrazol-5-yl)benzyl]benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-chloro-N-(pyridin-2-ylmethyl)-N-[4-(1H-tetrazol-5-yl)benzyl]benzenesulfonamide

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Technology Process of 4-chloro-N-(pyridin-2-ylmethyl)-N-[4-(1H-tetrazol-5-yl)benzyl]benzenesulfonamide

There total 4 articles about 4-chloro-N-(pyridin-2-ylmethyl)-N-[4-(1H-tetrazol-5-yl)benzyl]benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1191069-63-2
4-chloro-N-(4-cyanobenzyl)-N-(pyridin-2-ylmethyl)benzenesulfonamide

: 1191066-20-2
4-chloro-N-(pyridin-2-ylmethyl)-N-[4-(1H-tetrazol-5-yl)benzyl]benzenesulfonamide

Guidance literature:: With trimethylsilylazide; di(n-butyl)tin oxide; In toluene; at 90 ℃; for 18h;
DOI:10.1016/j.bmcl.2010.04.113

Reference yield:

: 3731-51-9
2-(Aminomethyl)pyridine

: 1191066-20-2
4-chloro-N-(pyridin-2-ylmethyl)-N-[4-(1H-tetrazol-5-yl)benzyl]benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 16 h / 0 - 20 °C

2: potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 2 h / 80 °C

3: trimethylsilylazide; di(n-butyl)tin oxide / toluene / 18 h / 90 °C

With trimethylsilylazide; di(n-butyl)tin oxide; potassium carbonate; triethylamine; sodium iodide; In dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 111195-91-6
4-chloro-N-(pyridin-2-ylmethyl)benzenesulfonamide

: 1191066-20-2
4-chloro-N-(pyridin-2-ylmethyl)-N-[4-(1H-tetrazol-5-yl)benzyl]benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 2 h / 80 °C

2: trimethylsilylazide; di(n-butyl)tin oxide / toluene / 18 h / 90 °C

With trimethylsilylazide; di(n-butyl)tin oxide; potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; toluene;