Technology Process of 5-(4-methoxy-benzoyl)-2-nitro-benzenesulfonamide
There total 6 articles about 5-(4-methoxy-benzoyl)-2-nitro-benzenesulfonamide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-amino-5-(4-methoxy-benzoyl)-benzenesulfonamide;
With
sodium perborate monohydrate; acetic acid;
at 50 ℃;
for 7h;
With
water; sodium hydroxide;
In
1,4-dioxane;
at 50 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: chlorosulfonic acid; sodium chloride / 160 °C
2.1: oxalyl dichloride / N,N-dimethyl-formamide / 0 - 20 °C
3.1: aluminum (III) chloride / dichloromethane / 0.17 h / 20 °C
3.2: 16 h / 20 °C
4.1: ammonia / dichloromethane; water / 0.17 h / 20 °C
5.1: ammonia / 1,4-dioxane; water / 6 h / 100 °C
6.1: sodium perborate monohydrate; acetic acid / 7 h / 50 °C
6.2: 1 h / 50 °C
With
chlorosulfonic acid; oxalyl dichloride; sodium perborate monohydrate; ammonia; acetic acid; sodium chloride;
aluminum (III) chloride; N,N-dimethyl-formamide;
In
1,4-dioxane; dichloromethane; water;
3.1: Friedel Crafts Acylation / 3.2: Friedel Crafts Acylation;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: oxalyl dichloride / N,N-dimethyl-formamide / 0 - 20 °C
2.1: aluminum (III) chloride / dichloromethane / 0.17 h / 20 °C
2.2: 16 h / 20 °C
3.1: ammonia / dichloromethane; water / 0.17 h / 20 °C
4.1: ammonia / 1,4-dioxane; water / 6 h / 100 °C
5.1: sodium perborate monohydrate; acetic acid / 7 h / 50 °C
5.2: 1 h / 50 °C
With
oxalyl dichloride; sodium perborate monohydrate; ammonia; acetic acid;
aluminum (III) chloride; N,N-dimethyl-formamide;
In
1,4-dioxane; dichloromethane; water;
2.1: Friedel Crafts Acylation / 2.2: Friedel Crafts Acylation;
