9b-(2,6-dichloro-α-iminobenzyl)-4b-hydroxy-5-methylindeno<1,2-b>indole

Base Information

Chemical Name:9b-(2,6-dichloro-α-iminobenzyl)-4b-hydroxy-5-methylindeno<1,2-b>indole
CAS No.:137041-64-6
Molecular Formula:C₂₃H₂₄Cl₂N₂O
Molecular Weight:415.362
Hs Code.:

Synonyms:9b-(2,6-dichloro-α-iminobenzyl)-4b-hydroxy-5-methylindeno<1,2-b>indole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9b-(2,6-dichloro-α-iminobenzyl)-4b-hydroxy-5-methylindeno<1,2-b>indole

Chemical Property:

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Technology Process of 9b-(2,6-dichloro-α-iminobenzyl)-4b-hydroxy-5-methylindeno<1,2-b>indole

There total 7 articles about 9b-(2,6-dichloro-α-iminobenzyl)-4b-hydroxy-5-methylindeno<1,2-b>indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 137041-62-4
indeno-isoxazolo-indole propellane

: 1194-65-6
2,6-dichloro-benzonitrile

: 7428-85-5
N-methylindeno<1,2-b>indole

: 137041-64-6
9b-(2,6-dichloro-α-iminobenzyl)-4b-hydroxy-5-methylindeno<1,2-b>indole

Guidance literature:: With hydrogen; nickel; In methanol; Ambient temperature;

Reference yield:

: 55366-49-9
N-methyl-1,2,3,4,5,6-hexahydro-1-benzoazocine-2,6-dione

: 137041-64-6
9b-(2,6-dichloro-α-iminobenzyl)-4b-hydroxy-5-methylindeno<1,2-b>indole

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / 25percent HCl / methanol / 1 h / Heating

2: 33 percent / CHCl₃ / Heating

3: 57 percent / H₂ / Raney nickel / methanol / Ambient temperature

With hydrogenchloride; hydrogen; nickel; In methanol; chloroform;

Reference yield:

: 52751-31-2
4-methyl-1,2,3,4-tetrahydro-cyclopenta[b]indole

: 137041-64-6
9b-(2,6-dichloro-α-iminobenzyl)-4b-hydroxy-5-methylindeno<1,2-b>indole

Guidance literature:: Multi-step reaction with 6 steps

1: 78 percent / CHCl₃ / Heating

2: H₂ / Raney nickel / methanol / Ambient temperature

4: 86 percent / 25percent HCl / methanol / 1 h / Heating

5: 33 percent / CHCl₃ / Heating

6: 57 percent / H₂ / Raney nickel / methanol / Ambient temperature

With hydrogenchloride; hydrogen; nickel; In methanol; chloroform;