4-<α-(4,5-Tetramethylen-(2H)1,3-dithiol-2-yliden)-α-cyanomethyl>-nitrobenzen

Base Information

Chemical Name:4-<α-(4,5-Tetramethylen-(2H)1,3-dithiol-2-yliden)-α-cyanomethyl>-nitrobenzen
CAS No.:119882-35-8
Molecular Formula:C₁₅H₁₂N₂O₂S₂
Molecular Weight:316.404
Hs Code.:

Synonyms:4-<α-(4,5-Tetramethylen-(2H)1,3-dithiol-2-yliden)-α-cyanomethyl>-nitrobenzen

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-<α-(4,5-Tetramethylen-(2H)1,3-dithiol-2-yliden)-α-cyanomethyl>-nitrobenzen

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Technology Process of 4-<α-(4,5-Tetramethylen-(2H)1,3-dithiol-2-yliden)-α-cyanomethyl>-nitrobenzen

There total 1 articles about 4-<α-(4,5-Tetramethylen-(2H)1,3-dithiol-2-yliden)-α-cyanomethyl>-nitrobenzen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 555-21-5,34512-13-5,174848-08-9
4-Nitrophenylacetonitrile

: 59102-97-5
2-Methylthio-4,5-tetramethylen-1,3-dithiolium-iodid

: 119882-35-8
4-<α-(4,5-Tetramethylen-(2H)1,3-dithiol-2-yliden)-α-cyanomethyl>-nitrobenzen

Guidance literature:: With triethylamine; In propan-1-ol; for 1h; Heating;

Reference yield: 36.0%

: 119882-35-8
4-<α-(4,5-Tetramethylen-(2H)1,3-dithiol-2-yliden)-α-cyanomethyl>-nitrobenzen

: 119882-24-5
4-<α-(4,5-Tetramethylen-(2H)1,3-dithiol-2-yliden)-α-cyanomethyl>-anilin

Guidance literature:: With sodium dithionite; sodium carbonate; In 1,4-dioxane; water; at 50 ℃;

Reference yield:

: 119882-35-8
4-<α-(4,5-Tetramethylen-(2H)1,3-dithiol-2-yliden)-α-cyanomethyl>-nitrobenzen

: 4-<α-(4,5-Tetramethylen-(2H)1,3-dithiol-2-yliden)-α-cyanomethyl>-benzendiazonium-tetrafluoroborat

Guidance literature:: Multi-step reaction with 2 steps

1: 36 percent / Na₂S₂O₄, Na₂CO₃ / H₂O; dioxane / 50 °C

2: 1.) NaNO₂; 2.) NaBF₄ / 1.) AcOH, H₂O, 5 min, 10 deg C; 2.) 2 h

With sodium tetrafluoroborate; sodium dithionite; sodium carbonate; sodium nitrite; In 1,4-dioxane; water;