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Nα-Boc-L-phenylalanyl-L-prolyl-glycine methyl ester

Base Information Edit
  • Chemical Name:Nα-Boc-L-phenylalanyl-L-prolyl-glycine methyl ester
  • CAS No.:100008-17-1
  • Molecular Formula:C22H31N3O6
  • Molecular Weight:433.505
  • Hs Code.:
  • Mol file:100008-17-1.mol
N<sup>α</sup>-Boc-L-phenylalanyl-L-prolyl-glycine methyl ester

Synonyms:Nα-Boc-L-phenylalanyl-L-prolyl-glycine methyl ester

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Chemical Property of Nα-Boc-L-phenylalanyl-L-prolyl-glycine methyl ester Edit
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Technology Process of Nα-Boc-L-phenylalanyl-L-prolyl-glycine methyl ester

There total 6 articles about Nα-Boc-L-phenylalanyl-L-prolyl-glycine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; cooling;
Guidance literature:
Multi-step reaction with 2 steps
1.1: HCl / ethyl acetate; H2O / 0.5 h
1.2: 86 percent / Zn dust / tetrahydrofuran / 0.17 h / 20 °C
2.1: 87 percent / Fmoc-Cl; NMM / tetrahydrofuran / 0.5 h / -15 °C
With 4-methyl-morpholine; hydrogenchloride; (fluorenylmethoxy)carbonyl chloride; In tetrahydrofuran; water; ethyl acetate;
Guidance literature:
Multi-step reaction with 3 steps
1.1: 90 percent / Fmoc-Cl; NMM / tetrahydrofuran / 0.5 h / -15 °C
2.1: HCl / ethyl acetate; H2O / 0.5 h
2.2: 86 percent / Zn dust / tetrahydrofuran / 0.17 h / 20 °C
3.1: 87 percent / Fmoc-Cl; NMM / tetrahydrofuran / 0.5 h / -15 °C
With 4-methyl-morpholine; hydrogenchloride; (fluorenylmethoxy)carbonyl chloride; In tetrahydrofuran; water; ethyl acetate;
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