(S)-2-((S)-2-Amino-3-benzyloxy-propionylamino)-3-benzyloxy-propionic acid ethyl ester; hydrochloride

Base Information

Chemical Name:(S)-2-((S)-2-Amino-3-benzyloxy-propionylamino)-3-benzyloxy-propionic acid ethyl ester; hydrochloride
CAS No.:114950-75-3
Molecular Formula:C₂₂H₂₈N₂O₅*ClH
Molecular Weight:436.936
Hs Code.:

Synonyms:(S)-2-((S)-2-Amino-3-benzyloxy-propionylamino)-3-benzyloxy-propionic acid ethyl ester; hydrochloride

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Chemical Property of (S)-2-((S)-2-Amino-3-benzyloxy-propionylamino)-3-benzyloxy-propionic acid ethyl ester; hydrochloride

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Technology Process of (S)-2-((S)-2-Amino-3-benzyloxy-propionylamino)-3-benzyloxy-propionic acid ethyl ester; hydrochloride

There total 3 articles about (S)-2-((S)-2-Amino-3-benzyloxy-propionylamino)-3-benzyloxy-propionic acid ethyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.8%

: 114950-73-1
Boc-(Ser(Bzl))2-OEt

: 114950-75-3
(S)-2-((S)-2-Amino-3-benzyloxy-propionylamino)-3-benzyloxy-propionic acid ethyl ester; hydrochloride

Guidance literature:: With hydrogenchloride; In ethyl acetate; for 2h; Ambient temperature;
DOI:10.1016/S0040-4020(01)86893-9

Reference yield:

: 23680-31-1
BOC-O-benzyl-L-serine

: 114950-75-3
(S)-2-((S)-2-Amino-3-benzyloxy-propionylamino)-3-benzyloxy-propionic acid ethyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) CDI; 2.) Et₃N / 1.) THF, 1 h; 2.) THF, 20 h, RT

2: 98.8 percent / HCl / ethyl acetate / 2 h / Ambient temperature

With hydrogenchloride; triethylamine; 1,1'-carbonyldiimidazole; In ethyl acetate;
DOI:10.1016/S0040-4020(01)86893-9

Reference yield:

: 58178-57-7
L-O-(benzyl)serine ethyl ester hydrochloride

: 114950-75-3
(S)-2-((S)-2-Amino-3-benzyloxy-propionylamino)-3-benzyloxy-propionic acid ethyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) CDI; 2.) Et₃N / 1.) THF, 1 h; 2.) THF, 20 h, RT

2: 98.8 percent / HCl / ethyl acetate / 2 h / Ambient temperature

With hydrogenchloride; triethylamine; 1,1'-carbonyldiimidazole; In ethyl acetate;
DOI:10.1016/S0040-4020(01)86893-9