2,4-di-O-benzoyl-3-O-benzyl-6-O-(tert-butyldiphenylsilyl)-α-D-galactopyranosyl-(1->4)-1,2,3,6-tetra-O-benzoyl-α-D-mannopyranose

Base Information

Chemical Name:2,4-di-O-benzoyl-3-O-benzyl-6-O-(tert-butyldiphenylsilyl)-α-D-galactopyranosyl-(1->4)-1,2,3,6-tetra-O-benzoyl-α-D-mannopyranose
CAS No.:214195-12-7
Molecular Formula:C₇₇H₇₀O₁₇Si
Molecular Weight:1295.48
Hs Code.:

Synonyms:2,4-di-O-benzoyl-3-O-benzyl-6-O-(tert-butyldiphenylsilyl)-α-D-galactopyranosyl-(1->4)-1,2,3,6-tetra-O-benzoyl-α-D-mannopyranose

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Chemical Property of 2,4-di-O-benzoyl-3-O-benzyl-6-O-(tert-butyldiphenylsilyl)-α-D-galactopyranosyl-(1->4)-1,2,3,6-tetra-O-benzoyl-α-D-mannopyranose

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Technology Process of 2,4-di-O-benzoyl-3-O-benzyl-6-O-(tert-butyldiphenylsilyl)-α-D-galactopyranosyl-(1->4)-1,2,3,6-tetra-O-benzoyl-α-D-mannopyranose

There total 1 articles about 2,4-di-O-benzoyl-3-O-benzyl-6-O-(tert-butyldiphenylsilyl)-α-D-galactopyranosyl-(1->4)-1,2,3,6-tetra-O-benzoyl-α-D-mannopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 56994-11-7
1,2,3,6-Tetra-O-benzoyl-α-D-mannopyranose

: 189622-61-5
2,4-di-O-benzoyl-3-O-benzyl-6-O-(tert-butyldiphenylsilyl)-α-D-galactopyranosyl trichloroacetimidate

: 214195-12-7
2,4-di-O-benzoyl-3-O-benzyl-6-O-(tert-butyldiphenylsilyl)-α-D-galactopyranosyl-(1->4)-1,2,3,6-tetra-O-benzoyl-α-D-mannopyranose

: 2,4-di-O-benzoyl-3-O-benzyl-6-O-(tert-butyldiphenylsilyl)-β-D-galactopyranosyl-(1->4)-1,2,3,6-tetra-O-benzoyl-α-D-mannopyranose

Guidance literature:: With triethylsilyl trifluoromethyl sulfonate; In dichloromethane; at 0 ℃; for 1h;

Reference yield:

: 214195-12-7
2,4-di-O-benzoyl-3-O-benzyl-6-O-(tert-butyldiphenylsilyl)-α-D-galactopyranosyl-(1->4)-1,2,3,6-tetra-O-benzoyl-α-D-mannopyranose

: C₇₀H₆₄O₁₇Si

Guidance literature:: With hydrogen; palladium dihydroxide; In methanol; ethyl acetate; at 20 ℃; for 24h;

Reference yield:

: 214195-12-7
2,4-di-O-benzoyl-3-O-benzyl-6-O-(tert-butyldiphenylsilyl)-α-D-galactopyranosyl-(1->4)-1,2,3,6-tetra-O-benzoyl-α-D-mannopyranose

: C₅₄H₄₆O₁₇

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 20 percent Pd(OH)2/C / methanol; ethyl acetate / 24 h / 20 °C

2: HCl / methanol; CH₂Cl₂ / 24 h / 20 °C

With hydrogenchloride; hydrogen; palladium dihydroxide; In methanol; dichloromethane; ethyl acetate; 1: Hydrogenolysis / 2: Desilylation;