C₅₀H₆₂N₄O₇S₃Si

Base Information

Chemical Name:C₅₀H₆₂N₄O₇S₃Si
CAS No.:1132667-42-5
Molecular Formula:C₅₀H₆₂N₄O₇S₃Si
Molecular Weight:955.348
Hs Code.:

C<sub>50</sub>H<sub>62</sub>N<sub>4</sub>O<sub>7</sub>S<sub>3</sub>Si

Synonyms:C₅₀H₆₂N₄O₇S₃Si

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₀H₆₂N₄O₇S₃Si

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Technology Process of C₅₀H₆₂N₄O₇S₃Si

There total 13 articles about C₅₀H₆₂N₄O₇S₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1033814-13-9
(R)-2-(2-((tert-butoxycarbonylamino)methyl)thiazol-4-yl)-4-methyl-4,5-dihydrothiazole-4-carboxylic acid

: 1132667-41-4
C₅₁H₅₅NO₆SSi

: 1132667-42-5
C₅₀H₆₂N₄O₇S₃Si

Guidance literature:: C₅₁H₅₅NO₆SSi; With diethylamine; In acetonitrile; for 2h;

(R)-2-(2-((tert-butoxycarbonylamino)methyl)thiazol-4-yl)-4-methyl-4,5-dihydrothiazole-4-carboxylic acid; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetonitrile; for 2h; Concentration;

Reference yield:

: 1033814-13-9
(R)-2-(2-((tert-butoxycarbonylamino)methyl)thiazol-4-yl)-4-methyl-4,5-dihydrothiazole-4-carboxylic acid

: C₃₆H₄₅NO₄SSi

: 1132667-42-5
C₅₀H₆₂N₄O₇S₃Si

Guidance literature:: (R)-2-(2-((tert-butoxycarbonylamino)methyl)thiazol-4-yl)-4-methyl-4,5-dihydrothiazole-4-carboxylic acid; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; for 0.0833333h;

C₃₆H₄₅NO₄SSi; In dichloromethane; acetonitrile;
DOI:10.1021/ol900078k

Reference yield:

: 3695-77-0
triphenylmethanethiol

: 1132667-42-5
C₅₀H₆₂N₄O₇S₃Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / dichloromethane

1.2: 80 °C

2.1: N-ethyl-N,N-diisopropylamine; titanium tetrachloride / dichloromethane / -78 °C

3.1: 1H-imidazole / dichloromethane

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

5.1: diethylamine / acetonitrile / 2 h

5.2: 2 h

With 1H-imidazole; dmap; titanium tetrachloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetonitrile;