Z-2-[2-(4-chlorophenylselanyl)ethyl]-3-methylpent-2-en-4-ynoic acid amide

Base Information

Chemical Name:Z-2-[2-(4-chlorophenylselanyl)ethyl]-3-methylpent-2-en-4-ynoic acid amide
CAS No.:182227-63-0
Molecular Formula:C₁₄H₁₄ClNOSe
Molecular Weight:326.684
Hs Code.:

Synonyms:Z-2-[2-(4-chlorophenylselanyl)ethyl]-3-methylpent-2-en-4-ynoic acid amide

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Chemical Property of Z-2-[2-(4-chlorophenylselanyl)ethyl]-3-methylpent-2-en-4-ynoic acid amide

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Technology Process of Z-2-[2-(4-chlorophenylselanyl)ethyl]-3-methylpent-2-en-4-ynoic acid amide

There total 7 articles about Z-2-[2-(4-chlorophenylselanyl)ethyl]-3-methylpent-2-en-4-ynoic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (Z)-2-[2-(4-Chloro-phenylselanyl)-ethyl]-3-methyl-pent-2-en-4-ynoyl chloride

: 182227-63-0
Z-2-[2-(4-chlorophenylselanyl)ethyl]-3-methylpent-2-en-4-ynoic acid amide

Guidance literature:: With ammonia; Yield given;
DOI:10.1016/0040-4039(96)01317-2

Reference yield:

: 182227-61-8
Z-3-[1-methyl-3-(trimethylsilanyl)prop-2-ynylidene]tetrahydrofuran-2-one

: 182227-63-0
Z-2-[2-(4-chlorophenylselanyl)ethyl]-3-methylpent-2-en-4-ynoic acid amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / tetrahydrofuran / 1.5 h / Heating

1.2: tetrahydrofuran / 4 h / Heating

2.1: (COCl)2 / 20 °C

3.1: 2.3 g / aq. NH₄OH / tetrahydrofuran / 0.25 h / 0 °C

With ammonium hydroxide; oxalyl dichloride; sodium hydride; In tetrahydrofuran;
DOI:10.1021/jo005531k

Reference yield:

: 316129-39-2
Z-2-[2-(4-chlorophenylselanyl)ethyl]-3-methylpent-2-en-4-ynoic acid

: 182227-63-0
Z-2-[2-(4-chlorophenylselanyl)ethyl]-3-methylpent-2-en-4-ynoic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1: (COCl)2 / 20 °C

2: 2.3 g / aq. NH₄OH / tetrahydrofuran / 0.25 h / 0 °C

With ammonium hydroxide; oxalyl dichloride; In tetrahydrofuran;
DOI:10.1021/jo005531k