4,6-O-di-tert-butylsilanediyl-2,3-O-di-benzyl-1-O-(5-azidopenty)-α-D-galactopyranoside

Base Information

Chemical Name:4,6-O-di-tert-butylsilanediyl-2,3-O-di-benzyl-1-O-(5-azidopenty)-α-D-galactopyranoside
CAS No.:1453170-69-8
Molecular Formula:C₃₃H₄₉N₃O₆Si
Molecular Weight:611.854
Hs Code.:

Synonyms:4,6-O-di-tert-butylsilanediyl-2,3-O-di-benzyl-1-O-(5-azidopenty)-α-D-galactopyranoside

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Chemical Property of 4,6-O-di-tert-butylsilanediyl-2,3-O-di-benzyl-1-O-(5-azidopenty)-α-D-galactopyranoside

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Technology Process of 4,6-O-di-tert-butylsilanediyl-2,3-O-di-benzyl-1-O-(5-azidopenty)-α-D-galactopyranoside

There total 2 articles about 4,6-O-di-tert-butylsilanediyl-2,3-O-di-benzyl-1-O-(5-azidopenty)-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1200763-56-9
4-methylphenyl 2,3-di-O-benzyl-4,6-O-di-tert-butylsilanediyl-1-thio-β-D-galactopyranoside

: 170220-11-8
5-azido-1-pentanol

: 1453170-69-8
4,6-O-di-tert-butylsilanediyl-2,3-O-di-benzyl-1-O-(5-azidopenty)-α-D-galactopyranoside

Guidance literature:: 4-methylphenyl 2,3-di-O-benzyl-4,6-O-di-tert-butylsilanediyl-1-thio-β-D-galactopyranoside; 5-azido-1-pentanol; In dichloromethane; at 20 ℃; for 3h; Molecular sieve; Inert atmosphere;

With N-iodo-succinimide; trifluorormethanesulfonic acid; In diethyl ether; dichloromethane; at -40 - 0 ℃; for 1h; Inert atmosphere;

Reference yield: 86.0%

: C₃₅H₄₆O₅SSi

: 170220-11-8
5-azido-1-pentanol

: 1453170-69-8
4,6-O-di-tert-butylsilanediyl-2,3-O-di-benzyl-1-O-(5-azidopenty)-α-D-galactopyranoside

Guidance literature:: C₃₅H₄₆O₅SSi; 5-azido-1-pentanol; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere; Microwave irradiation;

With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -40 - 0 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201302540