(R)-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-2-(4-methoxybenzyloxy)butan-1-ol

Base Information

• Chemical Name: (R)-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-2-(4-methoxybenzyloxy)butan-1-ol
• CAS No.: 1206732-05-9
• Molecular Formula: C₁₇H₂₆O₅
• Molecular Weight: 310.39
• Mol file: 1206732-05-9.mol

Synonyms:(R)-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-2-(4-methoxybenzyloxy)butan-1-ol

Chemical Property of (R)-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-2-(4-methoxybenzyloxy)butan-1-ol

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of (R)-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-2-(4-methoxybenzyloxy)butan-1-ol

There total 1 articles about (R)-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-2-(4-methoxybenzyloxy)butan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

(S)-4-(2-((4R)-2-(4-methoxyphenyl)-1,3-dioxolan-4-yl)ethyl)-2,2-dimethyl-1,3-dioxolane (1206732-04-8) → (R)-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-2-(4-methoxybenzyloxy)butan-1-ol (1206732-05-9)

Guidance literature:

With diisobutylaluminium hydride; In dichloromethane; toluene; at 0 ℃; for 12h;

DOI:10.1016/j.tetasy.2009.10.030

Reference yield:

(R)-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-2-(4-methoxybenzyloxy)butan-1-ol (1206732-05-9) → C17H24O5 (1206732-06-0)

Guidance literature:

With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 - 0 ℃; for 3.25h;

DOI:10.1016/j.tetasy.2009.10.030

upstream raw materials:

(S)-4-(2-((4R)-2-(4-methoxyphenyl)-1,3-dioxolan-4-yl)ethyl)-2,2-dimethyl-1,3-dioxolane

Downstream raw materials:

C₁₇H₂₄O₅