bis(4-benzoylphenyl)chlorophenylmethane

Base Information

Chemical Name:bis(4-benzoylphenyl)chlorophenylmethane
CAS No.:102343-14-6
Molecular Formula:C₃₃H₂₃ClO₂
Molecular Weight:486.997
Hs Code.:

Synonyms:bis(4-benzoylphenyl)chlorophenylmethane

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Chemical Property of bis(4-benzoylphenyl)chlorophenylmethane

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Technology Process of bis(4-benzoylphenyl)chlorophenylmethane

There total 9 articles about bis(4-benzoylphenyl)chlorophenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 102343-19-1
bis(4-benzoylphenyl)phenylmethanol

: 102343-14-6
bis(4-benzoylphenyl)chlorophenylmethane

Guidance literature:: With thionyl chloride; for 6h; Ambient temperature;
DOI:10.1021/ja00273a034

Reference yield:

: 90-90-4
(4-bromophenyl)(phenyl)methanone

: 102343-14-6
bis(4-benzoylphenyl)chlorophenylmethane

Guidance literature:: Multi-step reaction with 5 steps

1: 91 percent / PCl₅ / 2 h / 150 °C

2: 56 percent / 6 h

3: 57 percent / 1.) n-BuLi / diethyl ether / 1.) -35 to -10 deg C, 2 h, 2.) -10 deg C, 2 h then room temp., overnight and at last reflux for 3 h

4: 69 percent / diluted hydrochloric acid / ethanol / 2 h / Heating

5: 76 percent / thionyl chloride / 6 h / Ambient temperature

With hydrogenchloride; n-butyllithium; thionyl chloride; phosphorus pentachloride; In diethyl ether; ethanol;
DOI:10.1021/ja00273a034

Reference yield:

: 28225-70-9
(4-bromophenyl)dimethoxyphenylmethane

: 102343-14-6
bis(4-benzoylphenyl)chlorophenylmethane

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / 1.) n-BuLi / diethyl ether / 1.) -35 to -10 deg C, 2 h, 2.) -10 deg C, 2 h then room temp., overnight and at last reflux for 3 h

2: 69 percent / diluted hydrochloric acid / ethanol / 2 h / Heating

3: 76 percent / thionyl chloride / 6 h / Ambient temperature

With hydrogenchloride; n-butyllithium; thionyl chloride; In diethyl ether; ethanol;
DOI:10.1021/ja00273a034