C₅₃H₆₇ClF₂N₂O₁₄

Base Information

Chemical Name:C₅₃H₆₇ClF₂N₂O₁₄
CAS No.:869317-91-9
Molecular Formula:C₅₃H₆₇ClF₂N₂O₁₄
Molecular Weight:1029.57
Hs Code.:

C<sub>53</sub>H<sub>67</sub>ClF<sub>2</sub>N<sub>2</sub>O<sub>14</sub>

Synonyms:C₅₃H₆₇ClF₂N₂O₁₄

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Chemical Property of C₅₃H₆₇ClF₂N₂O₁₄

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Technology Process of C₅₃H₆₇ClF₂N₂O₁₄

There total 5 articles about C₅₃H₆₇ClF₂N₂O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 869317-90-8
C₅₃H₆₉ClF₂N₂O₁₄

: 869317-91-9
C₅₃H₆₇ClF₂N₂O₁₄

Guidance literature:: With dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride; In dichloromethane; at -78 ℃; for 1h;
DOI:10.1016/j.bmc.2005.06.003

Reference yield:

: 869317-88-4
C₆₉H₈₉ClN₂O₁₉S

: 869317-91-9
C₅₃H₆₇ClF₂N₂O₁₄

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / diethylaminosulfur trifluoride / CH₂Cl₂ / 72 h / 20 °C

2: 88 percent / hydrochloric acid / methanol / 1.5 h / 50 °C

3: 89 percent / DMSO; (CF₃CO)2O; Et₃N / CH₂Cl₂ / 1 h / -78 °C

With hydrogenchloride; diethylamino-sulfur trifluoride; dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2005.06.003

Reference yield:

: 869317-87-3
C₆₈H₉₁ClN₂O₁₉

: 869317-91-9
C₅₃H₆₇ClF₂N₂O₁₄

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / NaH; MeI / 4.5 h / 60 °C

2: 63 percent / diethylaminosulfur trifluoride / CH₂Cl₂ / 72 h / 20 °C

3: 88 percent / hydrochloric acid / methanol / 1.5 h / 50 °C

4: 89 percent / DMSO; (CF₃CO)2O; Et₃N / CH₂Cl₂ / 1 h / -78 °C

With hydrogenchloride; diethylamino-sulfur trifluoride; sodium hydride; dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride; methyl iodide; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2005.06.003