4-amino-4-p-chlorophenyl-5,6,7,8-tetrahydro-thieno<2,3-b>quinolin-2-carbonylazide

Base Information

Chemical Name:4-amino-4-p-chlorophenyl-5,6,7,8-tetrahydro-thieno<2,3-b>quinolin-2-carbonylazide
CAS No.:136920-47-3
Molecular Formula:C₁₈H₁₄ClN₅OS
Molecular Weight:383.861
Hs Code.:

Synonyms:4-amino-4-p-chlorophenyl-5,6,7,8-tetrahydro-thieno<2,3-b>quinolin-2-carbonylazide

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Chemical Property of 4-amino-4-p-chlorophenyl-5,6,7,8-tetrahydro-thieno<2,3-b>quinolin-2-carbonylazide

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Technology Process of 4-amino-4-p-chlorophenyl-5,6,7,8-tetrahydro-thieno<2,3-b>quinolin-2-carbonylazide

There total 4 articles about 4-amino-4-p-chlorophenyl-5,6,7,8-tetrahydro-thieno<2,3-b>quinolin-2-carbonylazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 136920-19-9
3-amino-4-(4'-chlorophenyl)-5,6,7,8-tetrahydro-thieno<2,3-b>quinoline-2-carbohydrazide

: 136920-47-3
4-amino-4-p-chlorophenyl-5,6,7,8-tetrahydro-thieno<2,3-b>quinolin-2-carbonylazide

Guidance literature:: With sodium nitrite; In acetic acid; Ambient temperature;

Reference yield:

: 83236-51-5
2-mercapto-4-(4-chlorophenyl)-5,6,7,8-tetrahydroquinoline-3-carbonitrile

: 136920-47-3
4-amino-4-p-chlorophenyl-5,6,7,8-tetrahydro-thieno<2,3-b>quinolin-2-carbonylazide

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / sodium acetate / ethanol / 2 h / Heating

2: 95 percent / hydrazine hydrate / ethanol / 4 h / Heating

3: 60 percent / K₂CO₃ / ethanol / 2 h / Heating

4: 83 percent / sodium nitrite / acetic acid / Ambient temperature

With sodium acetate; potassium carbonate; hydrazine hydrate; sodium nitrite; In ethanol; acetic acid;

Reference yield:

: 94833-55-3
ethyl <4-(4'-chlorophenyl)-3-cyano-5,6,7,8-tetrahydro-2-quinolinylthio>acetate

: 136920-47-3
4-amino-4-p-chlorophenyl-5,6,7,8-tetrahydro-thieno<2,3-b>quinolin-2-carbonylazide

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / hydrazine hydrate / ethanol / 4 h / Heating

2: 60 percent / K₂CO₃ / ethanol / 2 h / Heating

3: 83 percent / sodium nitrite / acetic acid / Ambient temperature

With potassium carbonate; hydrazine hydrate; sodium nitrite; In ethanol; acetic acid;