bromo[2-(3,3-dimethylbutyl)diazenido-N]bis[ethylenebis(diphenylphosphine)]molybdenum

Base Information

Chemical Name:bromo[2-(3,3-dimethylbutyl)diazenido-N]bis[ethylenebis(diphenylphosphine)]molybdenum
CAS No.:73153-18-1
Molecular Formula:C₅₈H₆₁BrMoN₂P₄
Molecular Weight:1085.87
Hs Code.:

Synonyms:bromo[2-(3,3-dimethylbutyl)diazenido-N]bis[ethylenebis(diphenylphosphine)]molybdenum

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bromo[2-(3,3-dimethylbutyl)diazenido-N]bis[ethylenebis(diphenylphosphine)]molybdenum

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Technology Process of bromo[2-(3,3-dimethylbutyl)diazenido-N]bis[ethylenebis(diphenylphosphine)]molybdenum

There total 1 articles about bromo[2-(3,3-dimethylbutyl)diazenido-N]bis[ethylenebis(diphenylphosphine)]molybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: trans-bisdinitrogenbis(1,2-diphenylphosphinoethane)molybdenum⁽⁰⁾

: 1647-23-0
3,3-dimethylbutyl bromide

: 73153-18-1
bromo[2-(3,3-dimethylbutyl)diazenido-N]bis[ethylenebis(diphenylphosphine)]molybdenum

Guidance literature:: In benzene; byproducts: N2; N2, at ambient temp. for 48 h in the dark; volume reduced, MeOH added, stirred for 1 h, evapd. to dryness, EtOH added, swirled for 0.1 h, filtered, filtrate stored for 48 h, filtered off,dried in vacuo; elem. anal.;
DOI:10.1021/ja00523a016

Reference yield: 93.1%

: tetrafluoroboric acid

: 73153-18-1
bromo[2-(3,3-dimethylbutyl)diazenido-N]bis[ethylenebis(diphenylphosphine)]molybdenum

: bromo[2-(3,3-dimethylbutyl)hydrazido-N]bis[ethylenebis(diphenylphosphine)]molybdenum tetrafluoroborate

Guidance literature:: In ethanol; benzene; N2, aq. HBF4 in EtOH added to a soln. of Mo-compound in benzene, heptane added over 1 h under stirring, stirred overnight; filtered, washed (ethanol/heptane), dried in vacuo; elem. anal.;
DOI:10.1021/ja00523a016