(2E)-3-(1-trityl-1H-imidazol-4-yl)prop-2-enyl propynoate

Base Information

Chemical Name:(2E)-3-(1-trityl-1H-imidazol-4-yl)prop-2-enyl propynoate
CAS No.:1300748-84-8
Molecular Formula:C₂₈H₂₂N₂O₂
Molecular Weight:418.495
Hs Code.:

Synonyms:(2E)-3-(1-trityl-1H-imidazol-4-yl)prop-2-enyl propynoate

Suppliers and Price of (2E)-3-(1-trityl-1H-imidazol-4-yl)prop-2-enyl propynoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2E)-3-(1-trityl-1H-imidazol-4-yl)prop-2-enyl propynoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2E)-3-(1-trityl-1H-imidazol-4-yl)prop-2-enyl propynoate

There total 4 articles about (2E)-3-(1-trityl-1H-imidazol-4-yl)prop-2-enyl propynoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 199007-50-6
1-(1-Trityl-1H-imidazol4-yl)propen-3-ol

: 471-25-0
Propiolic acid

: 1300748-84-8
(2E)-3-(1-trityl-1H-imidazol-4-yl)prop-2-enyl propynoate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/c0ob00657b

Reference yield:

: 112606-55-0
C₂₆H₂₂N₂O₂

: 1300748-84-8
(2E)-3-(1-trityl-1H-imidazol-4-yl)prop-2-enyl propynoate

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 - 20 °C / Inert atmosphere

With dmap; diisobutylaluminium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1039/c0ob00657b

Reference yield:

: 104-98-3
urocanic acid

: 1300748-84-8
(2E)-3-(1-trityl-1H-imidazol-4-yl)prop-2-enyl propynoate

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid; magnesium sulfate / Reflux

2: triethylamine / N,N-dimethyl-formamide

3: diisobutylaluminium hydride

4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 - 20 °C / Inert atmosphere

With dmap; sulfuric acid; diisobutylaluminium hydride; magnesium sulfate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide; 1: Fischer esterification;
DOI:10.1039/c0ob00657b