(2,6-Dihydroxy-4-methoxy-phenyl)-(2,4-dihydroxy-6-methyl-phenyl)-methanone

Base Information

• Chemical Name: (2,6-Dihydroxy-4-methoxy-phenyl)-(2,4-dihydroxy-6-methyl-phenyl)-methanone
• CAS No.: 60556-46-9
• Molecular Formula: C₁₅H₁₄O₆
• Molecular Weight: 290.273

Synonyms:(2,6-Dihydroxy-4-methoxy-phenyl)-(2,4-dihydroxy-6-methyl-phenyl)-methanone

Chemical Property of (2,6-Dihydroxy-4-methoxy-phenyl)-(2,4-dihydroxy-6-methyl-phenyl)-methanone

Chemical Property:

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Technology Process of (2,6-Dihydroxy-4-methoxy-phenyl)-(2,4-dihydroxy-6-methyl-phenyl)-methanone

There total 5 articles about (2,6-Dihydroxy-4-methoxy-phenyl)-(2,4-dihydroxy-6-methyl-phenyl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl-2,6-dihydroxy-4-methoxybenzoate (19722-76-0) → (2,6-Dihydroxy-4-methoxy-phenyl)-(2,4-dihydroxy-6-methyl-phenyl)-methanone (60556-46-9)

Guidance literature:

Multi-step reaction with 4 steps

1: K₂CO₃ / hexamethylphosphoric acid triamide

2: aq. KOH / ethane-1,2-diol

3: (CF₃CO)2O

4: H₂ / Pd-C

With potassium hydroxide; hydrogen; potassium carbonate; trifluoroacetic anhydride; palladium on activated charcoal; In N,N,N,N,N,N-hexamethylphosphoric triamide; ethylene glycol;

DOI:10.1021/ja00433a053

Reference yield:

2,6-Dibenzyloxy-4-methoxybenzoesaeure-methylester (60556-50-5) → (2,6-Dihydroxy-4-methoxy-phenyl)-(2,4-dihydroxy-6-methyl-phenyl)-methanone (60556-46-9)

Guidance literature:

Multi-step reaction with 3 steps

1: aq. KOH / ethane-1,2-diol

2: (CF₃CO)2O

3: H₂ / Pd-C

With potassium hydroxide; hydrogen; trifluoroacetic anhydride; palladium on activated charcoal; In ethylene glycol;

DOI:10.1021/ja00433a053

Reference yield:

(2,6-Bis-benzyloxy-4-methoxy-phenyl)-(2,4-bis-benzyloxy-6-methyl-phenyl)-methanone (60556-52-7) → (2,6-Dihydroxy-4-methoxy-phenyl)-(2,4-dihydroxy-6-methyl-phenyl)-methanone (60556-46-9)

Guidance literature:

With hydrogen; palladium on activated charcoal;

DOI:10.1021/ja00433a053

upstream raw materials:

(2,6-Bis-benzyloxy-4-methoxy-phenyl)-(2,4-bis-benzyloxy-6-methyl-phenyl)-methanone

methyl-2,6-dihydroxy-4-methoxybenzoate

(((5-methyl-1,3-phenylene)bis(oxy))bis(methylene))dibenzene

2,6-Dibenzyloxy-4-methoxybenzoesaeure-methylester

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