tert-butyl 2,2'-(4-(azidocarbonyl)-1,2-phenylene)bis(oxy)bis(ethane-2,1-diyl)bis(methylcarbamate)

Base Information

Chemical Name:tert-butyl 2,2'-(4-(azidocarbonyl)-1,2-phenylene)bis(oxy)bis(ethane-2,1-diyl)bis(methylcarbamate)
CAS No.:1228790-66-6
Molecular Formula:C₂₃H₃₅N₅O₇
Molecular Weight:493.56
Hs Code.:

Synonyms:tert-butyl 2,2'-(4-(azidocarbonyl)-1,2-phenylene)bis(oxy)bis(ethane-2,1-diyl)bis(methylcarbamate)

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Chemical Property of tert-butyl 2,2'-(4-(azidocarbonyl)-1,2-phenylene)bis(oxy)bis(ethane-2,1-diyl)bis(methylcarbamate)

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Technology Process of tert-butyl 2,2'-(4-(azidocarbonyl)-1,2-phenylene)bis(oxy)bis(ethane-2,1-diyl)bis(methylcarbamate)

There total 5 articles about tert-butyl 2,2'-(4-(azidocarbonyl)-1,2-phenylene)bis(oxy)bis(ethane-2,1-diyl)bis(methylcarbamate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1228792-14-0
C₂₃H₃₅ClN₂O₇

: 1228790-66-6
tert-butyl 2,2'-(4-(azidocarbonyl)-1,2-phenylene)bis(oxy)bis(ethane-2,1-diyl)bis(methylcarbamate)

Guidance literature:: With sodium azide; In acetone; for 0.0833333h;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1228790-66-6
tert-butyl 2,2'-(4-(azidocarbonyl)-1,2-phenylene)bis(oxy)bis(ethane-2,1-diyl)bis(methylcarbamate)

Guidance literature:: Multi-step reaction with 5 steps

1.1: ethyl acetate / 2 h / 20 °C / Cooling with ice

2.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 40 °C / Inert atmosphere; Cooling with ice

3.1: sodium hydroxide / methanol / 20 °C

3.2: pH ~ 4

4.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.05 h / 20 °C

5.1: sodium azide / acetone / 0.08 h

With sodium azide; oxalyl dichloride; di-isopropyl azodicarboxylate; triphenylphosphine; sodium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; acetone;

Reference yield:

: 1228792-11-7
methyl 3,4-bis(2-(tert-butoxycarbonyl(methyl)amino)ethoxy)benzoate

: 1228790-66-6
tert-butyl 2,2'-(4-(azidocarbonyl)-1,2-phenylene)bis(oxy)bis(ethane-2,1-diyl)bis(methylcarbamate)

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / methanol / 20 °C

1.2: pH ~ 4

2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.05 h / 20 °C

3.1: sodium azide / acetone / 0.08 h

With sodium azide; oxalyl dichloride; sodium hydroxide; N,N-dimethyl-formamide; In methanol; dichloromethane; acetone;