C₂₈H₃₀ClF₃N₂O₅SSi

Base Information

Chemical Name:C₂₈H₃₀ClF₃N₂O₅SSi
CAS No.:959999-83-8
Molecular Formula:C₂₈H₃₀ClF₃N₂O₅SSi
Molecular Weight:627.156
Hs Code.:

C<sub>28</sub>H<sub>30</sub>ClF<sub>3</sub>N<sub>2</sub>O<sub>5</sub>SSi

Synonyms:C₂₈H₃₀ClF₃N₂O₅SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₃₀ClF₃N₂O₅SSi

Chemical Property:

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Technology Process of C₂₈H₃₀ClF₃N₂O₅SSi

There total 10 articles about C₂₈H₃₀ClF₃N₂O₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 929280-80-8
(1S)-1-(2-chloro-3-{[(1,1-dimethylethyl)(dimethyl)silyl]oxy}-phenyl)ethanol

: 959999-82-7
methyl 3-hydroxy-5-{5-[(trifluoromethyl)oxy]-1H-benzimidazol-1-yl}-2-thiophenecarboxylate

: 959999-83-8
C₂₈H₃₀ClF₃N₂O₅SSi

Guidance literature:: With di-tert-butyl-diazodicarboxylate; triphenylphosphine; In dichloromethane; for 1h;

Reference yield:

: 95668-21-6
1-bromo-2-nitro-4-(trifluoromethoxy)benzene

: 959999-83-8
C₂₈H₃₀ClF₃N₂O₅SSi

Guidance literature:: Multi-step reaction with 5 steps

1: caesium carbonate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 16 h / 60 °C

2: hydrogen / 5 % platinum on sulfided carbon / ethyl acetate / 36 h / 38002.6 Torr

3: pyridinium p-toluenesulfonate / 24 h

4: trifluoroacetic acid / chloroform / 2 h / 60 °C

5: di-tert-butyl-diazodicarboxylate; triphenylphosphine / dichloromethane / 1 h

With di-tert-butyl-diazodicarboxylate; hydrogen; pyridinium p-toluenesulfonate; caesium carbonate; triphenylphosphine; trifluoroacetic acid; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 5 % platinum on sulfided carbon; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; dichloromethane; chloroform; ethyl acetate; 1: Suzuki Coupling / 5: Mitsunobu reaction;

Reference yield:

: 2267-23-4
2-nitro-4-trifluoromethoxyaniline

: 959999-83-8
C₂₈H₃₀ClF₃N₂O₅SSi

Guidance literature:: Multi-step reaction with 6 steps

1: tert.-butylnitrite; copper(ll) bromide / acetonitrile / 1 h / 20 °C

2: caesium carbonate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 16 h / 60 °C

3: hydrogen / 5 % platinum on sulfided carbon / ethyl acetate / 36 h / 38002.6 Torr

4: pyridinium p-toluenesulfonate / 24 h

5: trifluoroacetic acid / chloroform / 2 h / 60 °C

6: di-tert-butyl-diazodicarboxylate; triphenylphosphine / dichloromethane / 1 h

With tert.-butylnitrite; di-tert-butyl-diazodicarboxylate; hydrogen; pyridinium p-toluenesulfonate; caesium carbonate; triphenylphosphine; trifluoroacetic acid; copper(ll) bromide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 5 % platinum on sulfided carbon; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; dichloromethane; chloroform; ethyl acetate; acetonitrile; 2: Suzuki Coupling / 6: Mitsunobu reaction;