5,5'-dibromo-7'-methoxy-1'-<(4-methylphenyl)sulfonyl>-3,4'-bi-1H-indole

Base Information

Chemical Name:5,5'-dibromo-7'-methoxy-1'-<(4-methylphenyl)sulfonyl>-3,4'-bi-1H-indole
CAS No.:95739-86-9
Molecular Formula:C₂₄H₁₈Br₂N₂O₃S
Molecular Weight:574.293
Hs Code.:

Synonyms:5,5'-dibromo-7'-methoxy-1'-<(4-methylphenyl)sulfonyl>-3,4'-bi-1H-indole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5,5'-dibromo-7'-methoxy-1'-<(4-methylphenyl)sulfonyl>-3,4'-bi-1H-indole

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Technology Process of 5,5'-dibromo-7'-methoxy-1'-<(4-methylphenyl)sulfonyl>-3,4'-bi-1H-indole

There total 4 articles about 5,5'-dibromo-7'-methoxy-1'-<(4-methylphenyl)sulfonyl>-3,4'-bi-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.7%

: 622-88-8,41931-18-4
4-bromophenylhydrazine hydrochloride

: 95739-85-8
5-bromo-7-methoxy-1-<(4-methylphenyl)sulfonyl>-1H-indole-4-acetaldehyde

: 95739-86-9
5,5'-dibromo-7'-methoxy-1'-<(4-methylphenyl)sulfonyl>-3,4'-bi-1H-indole

Guidance literature:: With sodium acetate; zinc(II) chloride; In ethanol; Heating;
DOI:10.1021/ja00296a018

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 95739-86-9
5,5'-dibromo-7'-methoxy-1'-<(4-methylphenyl)sulfonyl>-3,4'-bi-1H-indole

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) triethylamine, pyridinium bromide perbromide; 2.) triethylamine / 1,) pyridine, 0-5 deg C, 5 min; 2.) room t., overnight

3: 63.7 percent / sodium acetate, zinc chloride / ethanol / Heating

With sodium acetate; pyridinium hydrobromide perbromide; triethylamine; zinc(II) chloride; In ethanol;
DOI:10.1021/ja00296a018

Reference yield:

: 95739-84-7
N-(4-bromo-5,8-dihydro-2-methoxy-1-naphthalenyl)-4-methyl-benzenesulfonamide

: 95739-86-9
5,5'-dibromo-7'-methoxy-1'-<(4-methylphenyl)sulfonyl>-3,4'-bi-1H-indole

Guidance literature:: Multi-step reaction with 2 steps

2: 63.7 percent / sodium acetate, zinc chloride / ethanol / Heating

With sodium acetate; zinc(II) chloride; In ethanol;
DOI:10.1021/ja00296a018