η5-1-(2-methoxyphenyl)-2,3,4,5-tetramethylcyclopentadienyl chromium dichloride dimer

Base Information

Chemical Name:η5-1-(2-methoxyphenyl)-2,3,4,5-tetramethylcyclopentadienyl chromium dichloride dimer
CAS No.:934008-00-1
Molecular Formula:C₃₂H₃₈Cl₄Cr₂O₂
Molecular Weight:700.457
Hs Code.:

Synonyms:η5-1-(2-methoxyphenyl)-2,3,4,5-tetramethylcyclopentadienyl chromium dichloride dimer

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Chemical Property of η5-1-(2-methoxyphenyl)-2,3,4,5-tetramethylcyclopentadienyl chromium dichloride dimer

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Technology Process of η5-1-(2-methoxyphenyl)-2,3,4,5-tetramethylcyclopentadienyl chromium dichloride dimer

There total 1 articles about η5-1-(2-methoxyphenyl)-2,3,4,5-tetramethylcyclopentadienyl chromium dichloride dimer which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.1%

: 915782-00-2
1-(2-methoxyphenyl)-2,3,4,5-tetramethylcyclopentadiene

: 10025-73-7,16284-59-6
chromium(III) chloride

: 934008-00-1
η5-1-(2-methoxyphenyl)-2,3,4,5-tetramethylcyclopentadienyl chromium dichloride dimer

Guidance literature:: With n-BuLi; In tetrahydrofuran; hexane; (Ar); std. Schlenk technique; soln. of BuLi in hexane was added dropwiseto soln. of ligand in THF at -78°C; mixt. was stirred at room te mp. for 12 h; added to suspn. of CrCl3 in THF at room temp.; mixt. was stirred for 12 h; filtered; solvent removed (vac.); recrystd. (CH2Cl2/hexane, 1/2); elem. anal.;
DOI:10.1016/j.jorganchem.2006.11.047