N-[2-(1H-indole-3-yl)-2-oxoethyl]-2-(3,4-dimethoxy phenyl)-2-oxoacetamide

Base Information

Chemical Name:N-[2-(1H-indole-3-yl)-2-oxoethyl]-2-(3,4-dimethoxy phenyl)-2-oxoacetamide
CAS No.:1447331-31-8
Molecular Formula:C₂₀H₁₈N₂O₅
Molecular Weight:366.373
Hs Code.:

Synonyms:N-[2-(1H-indole-3-yl)-2-oxoethyl]-2-(3,4-dimethoxy phenyl)-2-oxoacetamide

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Chemical Property of N-[2-(1H-indole-3-yl)-2-oxoethyl]-2-(3,4-dimethoxy phenyl)-2-oxoacetamide

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Technology Process of N-[2-(1H-indole-3-yl)-2-oxoethyl]-2-(3,4-dimethoxy phenyl)-2-oxoacetamide

There total 2 articles about N-[2-(1H-indole-3-yl)-2-oxoethyl]-2-(3,4-dimethoxy phenyl)-2-oxoacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₀H₁₀N₂O*H⁽¹⁺⁾

: 4732-70-1
3,4-dimethoxyphenylglyoxylic acid

: 1447331-31-8
N-[2-(1H-indole-3-yl)-2-oxoethyl]-2-(3,4-dimethoxy phenyl)-2-oxoacetamide

Guidance literature:: 3,4-dimethoxyphenylglyoxylic acid; With 1,1'-carbonyldiimidazole; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 1h;

C₁₀H₁₀N₂O*H⁽¹⁺⁾; In 1-methyl-pyrrolidin-2-one; at 20 ℃;
DOI:10.1016/j.tetlet.2013.05.095

Reference yield:

: 1131-62-0
1-(3,4-dimethoxyphenyl)ethanone

: 1447331-31-8
N-[2-(1H-indole-3-yl)-2-oxoethyl]-2-(3,4-dimethoxy phenyl)-2-oxoacetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: selenium(IV) oxide; pyridine

2.1: 1,1'-carbonyldiimidazole / 1-methyl-pyrrolidin-2-one / 1 h / 20 °C

2.2: 20 °C

With pyridine; selenium(IV) oxide; 1,1'-carbonyldiimidazole; In 1-methyl-pyrrolidin-2-one;
DOI:10.1016/j.tetlet.2013.05.095

Reference yield: 51.0%

: 1447331-31-8
N-[2-(1H-indole-3-yl)-2-oxoethyl]-2-(3,4-dimethoxy phenyl)-2-oxoacetamide

: 1447330-82-6
3-(3,4-dimethoxyphenyl)-5-(1H-indole-3-yl)pyrazine-2(1H)-one

Guidance literature:: With ammonium acetate; In acetic acid; at 160 ℃; for 0.0666667h; Sealed tube; Microwave irradiation;
DOI:10.1016/j.tetlet.2013.05.095