Acetophenone, 3-amino-5-methyl- (6CI)

Base Information

• Chemical Name: Acetophenone, 3-amino-5-methyl- (6CI)
• CAS No.: 102877-45-2
• Molecular Formula: C₉H₁₁NO
• Molecular Weight: 149.192
• Mol file: 102877-45-2.mol

Synonyms:Acetophenone,3'-amino-5'-methyl- (6CI)

Chemical Property of Acetophenone, 3-amino-5-methyl- (6CI)

Chemical Property:

• PSA: 43.09000
• LogP: 2.36100

Purity/Quality:

1-(3-Amino-5-methyl-phenyl)-ethanone 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Acetophenone, 3-amino-5-methyl- (6CI)

There total 2 articles about Acetophenone, 3-amino-5-methyl- (6CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(3-methyl-5-nitro-phenyl)-ethanone (110149-52-5) → 1-(3-amino-5-methyl-phenyl)-ethanone (102877-45-2)

Guidance literature:

With ethanol; nickel; Hydrogenation;

Reference yield:

3-methyl-5-nitro-benzoyl chloride (100249-20-5) → 1-(3-amino-5-methyl-phenyl)-ethanone (102877-45-2)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether / Erwaermen des Reaktionsprodukts mit H₂SO₄ enthaltender wss.Essigsaeure

2: Raney nickel; ethanol / Hydrogenation

With diethyl ether; ethanol; nickel;

upstream raw materials:

1-(3-methyl-5-nitro-phenyl)-ethanone

3-methyl-5-nitro-benzoyl chloride