C₃₁H₄₅NO₁₂

Base Information

Chemical Name:C₃₁H₄₅NO₁₂
CAS No.:1554478-10-2
Molecular Formula:C₃₁H₄₅NO₁₂
Molecular Weight:623.698
Hs Code.:

C<sub>31</sub>H<sub>45</sub>NO<sub>12</sub>

Synonyms:C₃₁H₄₅NO₁₂

Suppliers and Price of C₃₁H₄₅NO₁₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of C₃₁H₄₅NO₁₂

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of C₃₁H₄₅NO₁₂

There total 26 articles about C₃₁H₄₅NO₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1554478-28-2
C₄₄H₆₅NO₁₃Si

: 1554478-10-2
C₃₁H₄₅NO₁₂

Guidance literature:: With palladium on activated charcoal; hydrogen; In methanol; at 20 ℃;
DOI:10.1016/j.tetlet.2013.12.106

Reference yield:

: C₄₇H₆₃NO₁₂Si

: 1554478-10-2
C₃₁H₄₅NO₁₂

Guidance literature:: With pyridine; pyridine hydrogenfluoride; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1021/acs.orglett.6b01235

Reference yield:

: (2R,3R)-3-(4-methoxybenzyloxy)-4,4-dimethyl-1-phenyl-5-(triethylsilyloxy)pentan-2-ol

: 1554478-10-2
C₃₁H₄₅NO₁₂

Guidance literature:: Multi-step reaction with 11 steps

1: dmap / benzene / 17 h / 20 °C / Inert atmosphere

2: pyridinium p-toluenesulfonate / methanol / 0.75 h / 20 °C / Inert atmosphere

3: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 0.75 h / 20 °C / Molecular sieve; Inert atmosphere

4: sodium chlorite; sodium dihydrogen phosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 17 h / 20 °C

5: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 18 h / 20 °C

6: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 1.17 h / 20 °C

7: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 2.5 h / 20 °C / Molecular sieve

8: tetrakis(triphenylphosphine) palladium⁽⁰⁾; phenylsilane / dichloromethane / 6 h / 20 °C

9: triethylamine; dmap; 2-methyl-6-nitrobenzoic anhydride / dichloromethane / 20.5 h / 20 °C

10: tetrakis(triphenylphosphine) palladium⁽⁰⁾; phenylsilane / dichloromethane / 3.67 h / 20 °C

11: pyridine hydrogenfluoride; pyridine / tetrahydrofuran / 2 h / 20 °C

With pyridine; dmap; sodium chlorite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrapropylammonium perruthennate; sodium dihydrogen phosphate; 2-methyl-but-2-ene; phenylsilane; 2-methyl-6-nitrobenzoic anhydride; pyridinium p-toluenesulfonate; pyridine hydrogenfluoride; 4-methylmorpholine N-oxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; methanol; dichloromethane; water; tert-butyl alcohol; benzene;
DOI:10.1021/acs.orglett.6b01235