Technology Process of 14-(4-methoxybenzyloxy)tetradecanal
There total 5 articles about 14-(4-methoxybenzyloxy)tetradecanal which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dimethyl sulfoxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
tetrahydrofuran;
at 20 ℃;
for 4h;
DOI:10.1002/ejoc.200800680
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / tetrahydrofuran; dimethyl sulfoxide; mineral oil / 1 h / 0 °C
1.2: 18.5 h / 0 - 20 °C
2.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane; dimethyl sulfoxide / 24 h / 0 - 20 °C
With
sodium hydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide; mineral oil;
DOI:10.1021/ol3017676
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: dimethylsulfide borane complex / tetrahydrofuran / 7 h / 0 - 20 °C
2.1: sodium hydride / tetrahydrofuran; dimethyl sulfoxide; mineral oil / 1 h / 0 °C
2.2: 18.5 h / 0 - 20 °C
3.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dichloromethane; dimethyl sulfoxide / 24 h / 0 - 20 °C
With
dimethylsulfide borane complex; sodium hydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide; mineral oil;
DOI:10.1021/ol3017676
