BOC-D-CYS(BZL)-OH

Base Information

• Chemical Name: BOC-D-CYS(BZL)-OH
• CAS No.: 102830-49-9
• Molecular Formula: C15H21 N O4 S
• Molecular Weight: 311.402
• Mol file: 102830-49-9.mol

Synonyms:S-Benzyl-N-(tert-butoxycarbonyl)-D-cysteine

Chemical Property of BOC-D-CYS(BZL)-OH

Chemical Property:

• Vapor Pressure: 4.54E-10mmHg at 25°C
• Melting Point: 64-65℃
• Refractive Index: 1.554
• Boiling Point: 481.2°C at 760 mmHg
• PKA: 3.58±0.10(Predicted)
• Flash Point: 244.8°C
• PSA: 100.93000
• Density: 1.201g/cm³
• LogP: 3.28860
• Storage Temp.: Store at RT.

Purity/Quality:

99% ^*data from raw suppliers

Boc-S-benzyl-D-cysteine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BOC-D-CYS(BZL)-OH

There total 1 articles about BOC-D-CYS(BZL)-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(tert-butyloxycarbonyl)-D-serine β-lactone (98541-64-1,132340-68-2,126330-77-6) + phenylmethanethiol (100-53-8) → N-tert-butyloxycarbonyl-(S)-benzyl-N-(tert-butyloxycarbonyl)-D-cysteine (102830-49-9)

Guidance literature:

phenylmethanethiol; With sodium hydride; In tetrahydrofuran; mineral oil;

N-(tert-butyloxycarbonyl)-D-serine β-lactone; In tetrahydrofuran;

DOI:10.1021/jm701555p

Reference yield: 100.0%

1-(2-(piperidin-4-yl)ethyl)piperidine (14759-09-2) + N-tert-butyloxycarbonyl-(S)-benzyl-N-(tert-butyloxycarbonyl)-D-cysteine (102830-49-9) → N-tert-butyloxycarbonyl-(S)-(benzyl)-D-cysteine-[4-(2-(1-piperidyl)ethyl)]piperidinenamide (911069-07-3)

Guidance literature:

In dichloromethane;

Reference yield: 95.0%

N-tert-butyl-N'-phenyl-S-phenylisothiourea + N-tert-butyloxycarbonyl-(S)-benzyl-N-(tert-butyloxycarbonyl)-D-cysteine (102830-49-9) → tert-butyl (2S)-[3-(benzylsulfanyl)-1-oxo-1-(phenylamino)propan-2-yl]carbamate

Guidance literature:

With iron(III)-acetylacetonate; In isopropyl alcohol; at 83 ℃; for 48h; regioselective reaction; Sealed tube;

DOI:10.1002/adsc.201700134

upstream raw materials:

N-(tert-butyloxycarbonyl)-D-serine β-lactone

phenylmethanethiol

Downstream raw materials:

N²-tosyl-N⁴-(N-t-BOC-S-benzyl-D-cysteinyl)-L-2,4-diaminobutyrate benzyl ester

S-(phenylmethyl)-D-cysteine ethyl ester hydrochloride

(S)-N-(1S,2R)-<3-<2-<<(1,1-dimethylethyl)amino>carbonyl>phenyl>-2-hydroxy-1-(phenylmethyl)propyl>-2-<(tert-butoxycarbonyl)amino>-3-(benzylthio)propanamide

N-[1 (S)-[(2,3-dihydrospiro[1H-indene-1,4'-piperidin]-1'-yl)carbonyl]-2-(phenylmethylthio)ethyl]carbamic acid 1,1-dimethylethyl ester

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