4-chloro-5-(4-chlorophenyl)-9-(4-chlorophenylmethylene)-2-methylthio-6,7,8,9-tetrahydropyrimido[4,5-b]quinoline

Base Information

Chemical Name:4-chloro-5-(4-chlorophenyl)-9-(4-chlorophenylmethylene)-2-methylthio-6,7,8,9-tetrahydropyrimido[4,5-b]quinoline
CAS No.:1145713-51-4
Molecular Formula:C₂₅H₁₈Cl₃N₃S
Molecular Weight:498.863
Hs Code.:

Synonyms:4-chloro-5-(4-chlorophenyl)-9-(4-chlorophenylmethylene)-2-methylthio-6,7,8,9-tetrahydropyrimido[4,5-b]quinoline

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Chemical Property of 4-chloro-5-(4-chlorophenyl)-9-(4-chlorophenylmethylene)-2-methylthio-6,7,8,9-tetrahydropyrimido[4,5-b]quinoline

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Technology Process of 4-chloro-5-(4-chlorophenyl)-9-(4-chlorophenylmethylene)-2-methylthio-6,7,8,9-tetrahydropyrimido[4,5-b]quinoline

There total 1 articles about 4-chloro-5-(4-chlorophenyl)-9-(4-chlorophenylmethylene)-2-methylthio-6,7,8,9-tetrahydropyrimido[4,5-b]quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1027003-75-3
5-(4-chlorophenyl)-9-(4-chlorophenylmethylene)-2-methylthio-6,7,8,9-tetrahydropyrimido[4,5-b]-quinolin-4-one

: 1145713-51-4
4-chloro-5-(4-chlorophenyl)-9-(4-chlorophenylmethylene)-2-methylthio-6,7,8,9-tetrahydropyrimido[4,5-b]quinoline

Guidance literature:: 5-(4-chlorophenyl)-9-(4-chlorophenylmethylene)-2-methylthio-6,7,8,9-tetrahydropyrimido[4,5-b]-quinolin-4-one; With trichlorophosphate; In 1,4-dioxane; for 3h; Reflux;

With water; In 1,4-dioxane; at 20 ℃; Cooling;
DOI:10.1016/j.ejmech.2008.03.022

Reference yield: 90.0%

: 1145713-51-4
4-chloro-5-(4-chlorophenyl)-9-(4-chlorophenylmethylene)-2-methylthio-6,7,8,9-tetrahydropyrimido[4,5-b]quinoline

: 1145713-66-1
5-(4-chlorophenyl)-9-(4-chlorophenylmethylene)-2,4-dihydrazino-6,7,8,9-tetrahydropyrimido[4,5-b]quinoline

Guidance literature:: With hydrazine hydrate; In 1,4-dioxane; ethanol; for 12h; Reflux;
DOI:10.1016/j.ejmech.2008.03.022 DOI:10.1080/10426500802167027

Reference yield: 80.0%

: 1145713-51-4
4-chloro-5-(4-chlorophenyl)-9-(4-chlorophenylmethylene)-2-methylthio-6,7,8,9-tetrahydropyrimido[4,5-b]quinoline

: 62-53-3
aniline

: 1145713-52-5
5-(4-chlorophenyl)-9-(chlorophenylmethylene)-4-phenylamino-2-methylthio-6,7,8,9-tetrahydropyrimido[4,5-b]quinoline

Guidance literature:: 4-chloro-5-(4-chlorophenyl)-9-(4-chlorophenylmethylene)-2-methylthio-6,7,8,9-tetrahydropyrimido[4,5-b]quinoline; aniline; With acetic acid; for 3h; Reflux;

With water;
DOI:10.1016/j.ejmech.2008.03.022