H-Gly-3-(Gly)2-ONp TFA

Base Information

Chemical Name:H-Gly-3-(Gly)2-ONp TFA
CAS No.:96195-01-6
Molecular Formula:C₂HF₃O₂*C₅₁H₆₂N₁₀O₁₅
Molecular Weight:1169.14
Hs Code.:

Synonyms:H-Gly-3-(Gly)2-ONp TFA

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Chemical Property of H-Gly-3-(Gly)2-ONp TFA

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Technology Process of H-Gly-3-(Gly)2-ONp TFA

There total 3 articles about H-Gly-3-(Gly)2-ONp TFA which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 96195-19-6
[2-((S)-5-Benzyloxycarbamoyl-2-{(S)-5-benzyloxycarbamoyl-2-[(S)-5-benzyloxycarbamoyl-2-(2-tert-butoxycarbonylamino-acetylamino)-pentanoylamino]-pentanoylamino}-pentanoylamino)-acetylamino]-acetic acid 4-nitro-phenyl ester

: 76-05-1
trifluoroacetic acid

: 96195-01-6
H-Gly-3-(Gly)2-ONp TFA

Guidance literature:: In dichloromethane; for 0.5h; Ambient temperature;
DOI:10.1021/jo00213a013

Reference yield:

: 96195-29-8
Boc-Gly-3-(Gly)2-OH

: 96195-01-6
H-Gly-3-(Gly)2-ONp TFA

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / pyridine, 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride / dimethylformamide / 36 h / Ambient temperature

2: 87 percent / CH₂Cl₂ / 0.5 h / Ambient temperature

With pyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00213a013

Reference yield:

: 96194-99-9
Boc-Gly-3-(Gly)2-OMe

: 96195-01-6
H-Gly-3-(Gly)2-ONp TFA

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / 1 N aq. NaOH / methanol / 4 h / Ambient temperature

2: 70 percent / pyridine, 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride / dimethylformamide / 36 h / Ambient temperature

3: 87 percent / CH₂Cl₂ / 0.5 h / Ambient temperature

With pyridine; sodium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00213a013